山东化工
山東化工
산동화공
SHANDONG CHEMICAL INDUSTRY
2011年
9期
44-45
,共2页
吴震生%李凡华%范兴山%王飞龙
吳震生%李凡華%範興山%王飛龍
오진생%리범화%범흥산%왕비룡
3-溴-2-羰基环己甲酰胺%电位滴定%格列奇特%测定
3-溴-2-羰基環己甲酰胺%電位滴定%格列奇特%測定
3-추-2-탄기배기갑선알%전위적정%격렬기특%측정
3 - bromo - 2 - oxo - cyclohexyl formamide%potentiometric%gliclazide%determination
测定了格列奇特中间体3-溴-2-羰基环己甲酰胺的含量。样品经氧气瓶分解后，有机物中的碳和氢被氧化，溴索转化成钾盐。用电位滴定法测定溴的含量。此种方法的检测范围很宽阔，相对误差小于1％。
測定瞭格列奇特中間體3-溴-2-羰基環己甲酰胺的含量。樣品經氧氣瓶分解後，有機物中的碳和氫被氧化，溴索轉化成鉀鹽。用電位滴定法測定溴的含量。此種方法的檢測範圍很寬闊，相對誤差小于1％。
측정료격렬기특중간체3-추-2-탄기배기갑선알적함량。양품경양기병분해후，유궤물중적탄화경피양화，추색전화성갑염。용전위적정법측정추적함량。차충방법적검측범위흔관활，상대오차소우1％。
A new determination method of the gliclazide form amide was developed. The sample was decomposed was buried to carbon dioxide, bromine compounded into titrated potentiometrically with standard solution of silver intermediate 3 - Bromo - 2 - oxo - eyelohexyl oxygen flask method. The carbon in the sample potassium bromide. The resulting bromide was nitrate. This method could be used in a large scale and the relative error was less than 1%.
