无机化学学报
無機化學學報
무궤화학학보
JOURNAL OF INORGANIC CHEMISTRY
2009年
11期
2048-2052
,共5页
谈国强%宋亚玉%苗鸿雁%博海洋%夏傲
談國彊%宋亞玉%苗鴻雁%博海洋%夏傲
담국강%송아옥%묘홍안%박해양%하오
十八烷基三氯硅烷(OTS)%自组装%铁酸铋薄膜%图案化
十八烷基三氯硅烷(OTS)%自組裝%鐵痠鉍薄膜%圖案化
십팔완기삼록규완(OTS)%자조장%철산필박막%도안화
octadecyltrichlorosilane(Ors)%self-assembly%BiFeO_3 films%micropatteming
采用短波紫外光(UV)对十八烷基j氯硅烷(OTS)自组装单分子层(SAMs)进行刻蚀,利用化学液相法在OTS-SAMs模板表面制备出铁酸铋(BiFeO_3)图案化薄膜.通过接触角、X射线衍射(XRD)、扫描电镜(SEM)、X射线能谱(EDS)等测试手段对OTS膜和BiFeO_3薄膜进行表征.结果表明:以OTS为模板利用化学液相法成功制备出边缘轮廓清晰、条纹宽度为10-20 μm的BiFeO_3图案化薄膜.
採用短波紫外光(UV)對十八烷基j氯硅烷(OTS)自組裝單分子層(SAMs)進行刻蝕,利用化學液相法在OTS-SAMs模闆錶麵製備齣鐵痠鉍(BiFeO_3)圖案化薄膜.通過接觸角、X射線衍射(XRD)、掃描電鏡(SEM)、X射線能譜(EDS)等測試手段對OTS膜和BiFeO_3薄膜進行錶徵.結果錶明:以OTS為模闆利用化學液相法成功製備齣邊緣輪廓清晰、條紋寬度為10-20 μm的BiFeO_3圖案化薄膜.
채용단파자외광(UV)대십팔완기j록규완(OTS)자조장단분자층(SAMs)진행각식,이용화학액상법재OTS-SAMs모판표면제비출철산필(BiFeO_3)도안화박막.통과접촉각、X사선연사(XRD)、소묘전경(SEM)、X사선능보(EDS)등측시수단대OTS막화BiFeO_3박막진행표정.결과표명:이OTS위모판이용화학액상법성공제비출변연륜곽청석、조문관도위10-20 μm적BiFeO_3도안화박막.
Different kinds of micro-patterns were fabricated within octadecyhrichlorosilane (OTS) self-assembled monolayers(SAMs) utilizing UV lithography. The BiFeO_3 pattern films have been formed on silanol SAMs by the chemical solution deposition(CSD). The crystal phase composition, microstructure and topography of the as-prepared films were characterized by contact angle tester, X-ray diffraction (XRD), scanning electron microscopy (SEM) and energy disperse spectroscopy (EDS). The large contrast between octadecyl regions and silanol regions suggests selective deposition of BiFeO_3 film on the silanol regions with deposited line width of 10-20 μm.