稀有金属材料与工程
稀有金屬材料與工程
희유금속재료여공정
RARE METAL MATERIALS AND ENGINEERNG
2010年
1期
122-125
,共4页
叶林森%谌继明%谢东华%王锡胜%许泽金%陈伟
葉林森%諶繼明%謝東華%王錫勝%許澤金%陳偉
협림삼%심계명%사동화%왕석성%허택금%진위
表面粗糙度%Be%CuCrZr合金%镀层%热等静压%扩散连接
錶麵粗糙度%Be%CuCrZr閤金%鍍層%熱等靜壓%擴散連接
표면조조도%Be%CuCrZr합금%도층%열등정압%확산련접
surface roughness%Be%CuCrZr alloy%coating%hot isostatic pressing%diffusion bonding
在不同表面粗糙度的Be侧镀Ti/Cu中间层,采用热等静压技术将铍与CuCrZr合金进行扩散连接.通过AES、SEM(EDS)、室温剪切试验和XRD等分析其镀层形貌及成分、界面特性与相结构.结果表明:9 μm Ti、35 μm Cu镀层带征较为均匀,影响扩散连接强度的元素较少,采用双靶单侧镀复合膜的工艺有利于减少Ti镀层的氧化;界面剪切强度明显提高,最高可达243 MPa,Be表面粗糙度的不同对强度影响不明显;Be-Ti连接强度高,剪切断裂均发生在Cu镀层.
在不同錶麵粗糙度的Be側鍍Ti/Cu中間層,採用熱等靜壓技術將鈹與CuCrZr閤金進行擴散連接.通過AES、SEM(EDS)、室溫剪切試驗和XRD等分析其鍍層形貌及成分、界麵特性與相結構.結果錶明:9 μm Ti、35 μm Cu鍍層帶徵較為均勻,影響擴散連接彊度的元素較少,採用雙靶單側鍍複閤膜的工藝有利于減少Ti鍍層的氧化;界麵剪切彊度明顯提高,最高可達243 MPa,Be錶麵粗糙度的不同對彊度影響不明顯;Be-Ti連接彊度高,剪切斷裂均髮生在Cu鍍層.
재불동표면조조도적Be측도Ti/Cu중간층,채용열등정압기술장피여CuCrZr합금진행확산련접.통과AES、SEM(EDS)、실온전절시험화XRD등분석기도층형모급성분、계면특성여상결구.결과표명:9 μm Ti、35 μm Cu도층대정교위균균,영향확산련접강도적원소교소,채용쌍파단측도복합막적공예유리우감소Ti도층적양화;계면전절강도명현제고,최고가체243 MPa,Be표면조조도적불동대강도영향불명현;Be-Ti련접강도고,전절단렬균발생재Cu도층.
Ti and Cu were used as interlayer materials, and the diffusion bonding of Be/CuCrZr alloys were carried out onto Be side by hot isostatic pressing. The four Be samples had different surface roughness. The coating, interface behavior and microstructure of the diffusion bonded alloys were studied by AES, SEM (EDS), room-temperature shear test and XRD. The results show that the Ti coating band (9 μm thickness) and the Cu coating band (35 μm thickness) are homogeneous, and few harmful ingredients are observed. Dual-target and single-side coating technology is favorable to reduce the Ti-coating oxidation. Shearing strength of the Be/CuCrZr interface is increased significantly, with the highest up to 243 MPa. But effect of the different surface roughness on the shearing strength is not obvious. The bonding strength of Be-Ti is high, and all the shear fracture of the samples occurs in the Cu layer.