中国药师
中國藥師
중국약사
CHINA PHARMACIST
2011年
4期
505-507
,共3页
芙蓉抗流感胶囊%高效液相色谱法%木芙蓉
芙蓉抗流感膠囊%高效液相色譜法%木芙蓉
부용항류감효낭%고효액상색보법%목부용
目的:建立芙蓉抗流感胶囊中槲皮素、山奈素、异鼠李素含量测定方法.方法:采用Waters Xbridge C18(250 mm×4.6 mm,5μm)色谱柱;以甲醇-0.4%磷酸水溶液为流动相梯度洗脱;流速为1.0 ml· min-1;检测波长为360 nm;柱温:25℃.结果:槲皮素、山奈素、异鼠李素的线性范围分别为63.4 ~634.0 μg(r =0.999 9),70.8~708.0 μg(r =0.999 8),45.8 ~458.0μg(r =0.9998);加样回收率分别为98.45%、98.79%与99.16%.结论:该方法简单、快速、准确,可用于芙蓉抗流感胶囊的质量控制.
目的:建立芙蓉抗流感膠囊中槲皮素、山奈素、異鼠李素含量測定方法.方法:採用Waters Xbridge C18(250 mm×4.6 mm,5μm)色譜柱;以甲醇-0.4%燐痠水溶液為流動相梯度洗脫;流速為1.0 ml· min-1;檢測波長為360 nm;柱溫:25℃.結果:槲皮素、山奈素、異鼠李素的線性範圍分彆為63.4 ~634.0 μg(r =0.999 9),70.8~708.0 μg(r =0.999 8),45.8 ~458.0μg(r =0.9998);加樣迴收率分彆為98.45%、98.79%與99.16%.結論:該方法簡單、快速、準確,可用于芙蓉抗流感膠囊的質量控製.
목적:건립부용항류감효낭중곡피소、산내소、이서리소함량측정방법.방법:채용Waters Xbridge C18(250 mm×4.6 mm,5μm)색보주;이갑순-0.4%린산수용액위류동상제도세탈;류속위1.0 ml· min-1;검측파장위360 nm;주온:25℃.결과:곡피소、산내소、이서리소적선성범위분별위63.4 ~634.0 μg(r =0.999 9),70.8~708.0 μg(r =0.999 8),45.8 ~458.0μg(r =0.9998);가양회수솔분별위98.45%、98.79%여99.16%.결론:해방법간단、쾌속、준학,가용우부용항류감효낭적질량공제.