化学试剂
化學試劑
화학시제
CHEMICAL REAGENTS
2010年
3期
261-262
,共2页
林彦飞%王小英%吴巧玲%林原斌
林彥飛%王小英%吳巧玲%林原斌
림언비%왕소영%오교령%림원빈
4-氨基吡啶%Sandmeyer反应%3,5-二溴吡啶
4-氨基吡啶%Sandmeyer反應%3,5-二溴吡啶
4-안기필정%Sandmeyer반응%3,5-이추필정
4-aminopyridine%Sandmeyer reaction%3,5-dibromopyridine
以易得的4-氨基吡啶为原料经过溴化、改进的Sandmeyer重氮化还原反应得到标题化合物,总收率可达36.8%.
以易得的4-氨基吡啶為原料經過溴化、改進的Sandmeyer重氮化還原反應得到標題化閤物,總收率可達36.8%.
이역득적4-안기필정위원료경과추화、개진적Sandmeyer중담화환원반응득도표제화합물,총수솔가체36.8%.
3,5-Dibromopyridine was synthesized from 4-aminopyridine by bromination with bromine,which was deaminized through the improved Sandmeyer reaction,with an overall yield of 36.8%.