无机化学学报
無機化學學報
무궤화학학보
JOURNAL OF INORGANIC CHEMISTRY
2007年
5期
923-927
,共5页
方建%杜贤龙%吕辉鸿%郭丹%赵继华%沈伟国
方建%杜賢龍%呂輝鴻%郭丹%趙繼華%瀋偉國
방건%두현룡%려휘홍%곽단%조계화%침위국
微乳液%Triton X-100%普鲁士蓝类配合物%纳米颗粒
微乳液%Triton X-100%普魯士藍類配閤物%納米顆粒
미유액%Triton X-100%보로사람류배합물%납미과립
microemulsion%Triton X-100%Prussian blue analogues%nanoparticle
Highly oriented cubic, hollow cubic and spherical nanoparticles of cobalt-iron Prussian blue analogues were synthesized in poly oxyethylene tertoctylphenyl ether (TritonX-100)/n-hexanol/cyclohexane microemulsion.The effects of the water-to-surfactant molar ratio (w), the reactant concentration and the reaction temperature on the morphology of cobalt-iron Prussian blue analogues were studied. The samples were characterized by transmission electron microscopy (TEM), field emission scan electron microscopy (FE-SEM), energy-dispersive X-ray spectroscopy (EDS), X-ray diffraction (XRD) and infrared spectroscopy (IR).
