CAJ | 학술논문

采用气相色谱法测定甲基磺酸钠酰氯化反应产物中甲基磺酰氯的含量，计算甲基磺酰氯的收率，从而选择和控制酰氯化过程的工艺条件．该法具有分析速度快、操作简便、重现性好、准确度高等特点，可应用于对甲基磺酸钠酰氯化生产甲基磺酰氯的中控分析．
채용기상색보법측정갑기광산납선록화반응산물중갑기광선록적함량，계산갑기광선록적수솔，종이선택화공제선록화과정적공예조건．해법구유분석속도쾌、조작간편、중현성호、준학도고등특점，가응용우대갑기광산납선록화생산갑기광선록적중공분석．
In the production of methanesulfonyl chloride from sodium methanesulfonic acid, the yield of methanesulfonyl chloride is determined through gas chromatography and calculated to help select and control the reaction conditions. This method is characterized by high speed analysis, simple operation, great reproducibility and high accuracy, and can be applied for the middle-controlled analysis of methanesulfonyl chloride in the acid chloride reaction.