原子能科学技术
原子能科學技術
원자능과학기술
ATOMIC ENERGY SCIENCE AND TECHNOLOGY
2001年
2期
116-120
,共5页
沙建军%郁金南%郁刚%韩华%罗金汉
沙建軍%鬱金南%鬱剛%韓華%囉金漢
사건군%욱금남%욱강%한화%라금한
准单畴%熔融织构YBCO超导体%临界电流密度%钉扎中心
準單疇%鎔融織構YBCO超導體%臨界電流密度%釘扎中心
준단주%용융직구YBCO초도체%림계전류밀도%정찰중심
采用熔融织构生长法(MTG)结合顶部籽晶工艺(TSP)制备了不同Y-211粒子含量的准单畴熔融织构的YBCO块材,样品致密度高,机械强度好。VSM测量结果表明:样品在30K、0.6T下,临界电流密度JC达到1.23×106A/cm2;在70K、2T下,JC为1.35×104A/cm2,且JC对磁场不敏感。SEM分析结果表明:Y-211相的掺杂能够改善织构样品的生长状况,同时,掺杂的Y-211粒子又能作为强的钉扎中心;所制备的样品中Y-211粒子分布越均匀,尺寸越小,其钉扎效果越好。
採用鎔融織構生長法(MTG)結閤頂部籽晶工藝(TSP)製備瞭不同Y-211粒子含量的準單疇鎔融織構的YBCO塊材,樣品緻密度高,機械彊度好。VSM測量結果錶明:樣品在30K、0.6T下,臨界電流密度JC達到1.23×106A/cm2;在70K、2T下,JC為1.35×104A/cm2,且JC對磁場不敏感。SEM分析結果錶明:Y-211相的摻雜能夠改善織構樣品的生長狀況,同時,摻雜的Y-211粒子又能作為彊的釘扎中心;所製備的樣品中Y-211粒子分佈越均勻,呎吋越小,其釘扎效果越好。
채용용융직구생장법(MTG)결합정부자정공예(TSP)제비료불동Y-211입자함량적준단주용융직구적YBCO괴재,양품치밀도고,궤계강도호。VSM측량결과표명:양품재30K、0.6T하,림계전류밀도JC체도1.23×106A/cm2;재70K、2T하,JC위1.35×104A/cm2,차JC대자장불민감。SEM분석결과표명:Y-211상적참잡능구개선직구양품적생장상황,동시,참잡적Y-211입자우능작위강적정찰중심;소제비적양품중Y-211입자분포월균균,척촌월소,기정찰효과월호。
The paper describes the method of melt-textured growth(MTG) witha top-seeded technique to prepare the quasi-single crystal domain YBCO bulk materials with various Y-211 particle contents. The obtained specimens have high density and good mechanical toughness. The JC of specimens reaches 1.23×106 A/cm2 under 0.6 T at 30 K and 1.35×104 A/cm2 under 2 T at 70 K. The SEM observation of specimens indicates that Y-211 particles can improve the quality of melt-textured YBCO superconductor. Combining the microstructures with JC measurements shows that the smaller the particle size and the more homogeneous the particle distribution is, the better the pinning effectiveness is.