二(α-肟基丙酸根)合铜(Ⅱ)的固相合成、表征及热分解
이(α-우기병산근)합동(Ⅱ)적고상합성、표정급열분해
SYNTHESIS, CHARACTERIZATION AND PYROLYSIS OF BIS(2-HYDROXYIMINOPROPANOATO) COPPER(Ⅱ) BY SOLID STATE REACTION
  • 万方数据
    无机化学学报 무궤화학학보
    JOURNAL OF INORGANIC CHEMISTRY
    1999年 5期 648-651 ,共4页

    刘扬中%张祖德%郑韬%余华明%刘清亮

    류양중%장조덕%정도%여화명%류청량

    固相反应%α-肟基丙酸%纳米微粒%氧化铜 固相反應%α-肟基丙痠%納米微粒%氧化銅
    고상반응%α-우기병산%납미미립%양화동
    solid reaction propanoic acid 2-(hydroxyimino) nanometer particles copper oxide


    Bis(2-hydroxyiminopropanoato) copper (Ⅱ) ([Cu(PAO)2]·2H2O) was synthesized by one step solid reaction between Cu(Ac)2·H2O and 2-hydroxyimino propanoic acid (HPAO) at 50℃.The complex was characterized by elemental analysis, IR, XRD, flourenscence spectrum and thermal analysis. XRD and TEM showed nanometer particles (about 20～30 nm) of CuO was prepared by pyrolysis of the complex at 300℃ in the air.
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