化学世界
化學世界
화학세계
CHEMICAL WORLD
2009年
7期
392-395,409
,共5页
古映莹%周琼华%周建良%钟世安%庄树新
古映瑩%週瓊華%週建良%鐘世安%莊樹新
고영형%주경화%주건량%종세안%장수신
钒%活化焙烧%酸浸%浸出率
釩%活化焙燒%痠浸%浸齣率
범%활화배소%산침%침출솔
vanadium%activated roasting%acid-leaching%leaching rate
对河南某钒矿进行了活化焙烧-酸浸实验,系统考察了添加剂种类与用量、焙烧温度、焙烧时间、浸取酸度、液固比、浸取温度及时间对钒浸取率的影响.实验结果表明:焙烧过程中,采用氧化钙为添加剂,控制添加量为10%,850~900℃下焙烧3 h,矿样的活化效果较好;酸浸过程中,硫酸酸度为5%,液固比为2.5:1,70~80℃,漫出3 h的条件下,钒的浸出率最高,可达80%以上.
對河南某釩礦進行瞭活化焙燒-痠浸實驗,繫統攷察瞭添加劑種類與用量、焙燒溫度、焙燒時間、浸取痠度、液固比、浸取溫度及時間對釩浸取率的影響.實驗結果錶明:焙燒過程中,採用氧化鈣為添加劑,控製添加量為10%,850~900℃下焙燒3 h,礦樣的活化效果較好;痠浸過程中,硫痠痠度為5%,液固比為2.5:1,70~80℃,漫齣3 h的條件下,釩的浸齣率最高,可達80%以上.
대하남모범광진행료활화배소-산침실험,계통고찰료첨가제충류여용량、배소온도、배소시간、침취산도、액고비、침취온도급시간대범침취솔적영향.실험결과표명:배소과정중,채용양화개위첨가제,공제첨가량위10%,850~900℃하배소3 h,광양적활화효과교호;산침과정중,류산산도위5%,액고비위2.5:1,70~80℃,만출3 h적조건하,범적침출솔최고,가체80%이상.
Vanadium was recovered by a new roasting-acid leaching process from vanadium ore in Henan Province. The influence of category of additive, percentage of additive, roasting temperature, roasting time, acid concentration, solid-to-liquid ratio, leaching temperature and leaching time upon leaching rate was investigated. The experimental results showed that the vanadium ore was well activated when calcium oxide was used as additive, the percentage of additive was 10% and the ore was roasted at 850~900℃ for 3 hours. In acid leaching process, the leaching rate was above 80% when the ore was leached at 70~80℃for 3 hours, the add concentration was 5% and the solid-to-liquid ratio was 2.5 : 1.