合成化学
閤成化學
합성화학
CHINESE JOURNAL OF SYNTHETIC CHEMISTRY
2009年
6期
736-738
,共3页
薁%1-甲酰基薁%吲哚衍生物%合成
薁%1-甲酰基薁%吲哚衍生物%閤成
욱%1-갑선기욱%신타연생물%합성
azulene%1-formoylazulene%indole derivative%synthesis
1-甲酰基薁-3-甲酸甲酯和2,3,3-三甲基-3H-吲哚衍生物发生缩合反应,合成了一系列3,3-二甲基-2-(3-甲基薁乙烯基)-3H-吲哚衍生物,收率48%～64%,其结构经~1H NMR,IR和元素分析表征.
1-甲酰基薁-3-甲痠甲酯和2,3,3-三甲基-3H-吲哚衍生物髮生縮閤反應,閤成瞭一繫列3,3-二甲基-2-(3-甲基薁乙烯基)-3H-吲哚衍生物,收率48%～64%,其結構經~1H NMR,IR和元素分析錶徵.
1-갑선기욱-3-갑산갑지화2,3,3-삼갑기-3H-신타연생물발생축합반응,합성료일계렬3,3-이갑기-2-(3-갑기욱을희기)-3H-신타연생물,수솔48%～64%,기결구경~1H NMR,IR화원소분석표정.
A series of 3,3-dimethyl-2-(3-methylazulenevinyl)-3H-indole derivatives in yields of 48%～64% were synthesized by condensation of 1-formoyl-3-methyl-azulene with 2,3,3-trimethyl-3H-indole derivatives. The structures were characterized by ~1H NMR, IR and elemental analysis.
