中医药导报
中醫藥導報
중의약도보
GUIDING JOURNAL OF TCM
2009年
7期
85-86
,共2页
李镜友%陈军%罗巧红%沈玉霞%李国强%胡晓庆%陈研
李鏡友%陳軍%囉巧紅%瀋玉霞%李國彊%鬍曉慶%陳研
리경우%진군%라교홍%침옥하%리국강%호효경%진연
HPLC%蒸发光散射%益气温阳胶囊%黄芪甲苷
HPLC%蒸髮光散射%益氣溫暘膠囊%黃芪甲苷
HPLC%증발광산사%익기온양효낭%황기갑감
HPLC%Evaporative light scattering%Yiqiwenyang capsule%Astragaloside
目的:建立益气温阳胶囊中黄芪甲苷的含量测定方法.方法:采用HPLC-蒸发光散射检测法,以Hypersil BDS C18为色谱柱,以乙腈-水(32:68)为流动相,蒸发光散射检测器.结果:黄芪甲苷平均加样回收率为96.67%,RSD%为0.79%.结论:所建方法灵敏、准确,重现性好,能有效控制益气温阳胶囊的质量.
目的:建立益氣溫暘膠囊中黃芪甲苷的含量測定方法.方法:採用HPLC-蒸髮光散射檢測法,以Hypersil BDS C18為色譜柱,以乙腈-水(32:68)為流動相,蒸髮光散射檢測器.結果:黃芪甲苷平均加樣迴收率為96.67%,RSD%為0.79%.結論:所建方法靈敏、準確,重現性好,能有效控製益氣溫暘膠囊的質量.
목적:건립익기온양효낭중황기갑감적함량측정방법.방법:채용HPLC-증발광산사검측법,이Hypersil BDS C18위색보주,이을정-수(32:68)위류동상,증발광산사검측기.결과:황기갑감평균가양회수솔위96.67%,RSD%위0.79%.결론:소건방법령민、준학,중현성호,능유효공제익기온양효낭적질량.
Objective: To establish the determination method for astragaloside in Yiqiwenyang capsule.Methods:HPLC-evap-orative light scattering detection method method was used with Hypersil BDS C18 as chromatographic eolumn,acetonitrile-wa-ter(32:68) as mobile phase, evaporative light scattering detection machine. Result: The average spotting recovery of astragalo-side was 96.67%, RSD%=0.79%.Conclnsion: The method is sensitive, accurate with good reproducibility, can be control the quality of Yiqiwenyang capsule.
