现代技术陶瓷
現代技術陶瓷
현대기술도자
ADVANCED CERAMICS
2011年
4期
3-7
,共5页
刘博%韩亚苓%朴新欣%肖久寒%王振
劉博%韓亞苓%樸新訢%肖久寒%王振
류박%한아령%박신흔%초구한%왕진
衬瓷层%预渗入法衬瓷%坯体%造孔剂%预烧%烧结
襯瓷層%預滲入法襯瓷%坯體%造孔劑%預燒%燒結
츤자층%예삼입법츤자%배체%조공제%예소%소결
lining ereamic layer%pre -permeating lining ceramics%green body%porous agent%pre - burn
传统陶瓷涂层在质量、能耗、以及环保等方面都存在一定的问题,针对这一现象,提出了预渗入法制备陶瓷涂层技术。即预先在坯体表面造出孔洞,将陶瓷复合粉料预先渗入到坯体表面的孔洞中,通过烧结,在金属表面制备一层具有优异耐磨性的衬瓷层。研究了造孔剂加入量、预烧工艺等参数对孔分布的影响规律,利用扫描电镜分析了预烧后坯体的孔洞分布规律和烧结后衬瓷层的显微组织,实验结果表明:造孔剂的加入量(淀粉)为10%、预烧工艺参数为400℃×1h时,坯体中孔的分布较为均匀,孔径大小适合纳米氧化锆的预渗入;预渗入法获得的衬瓷层厚度为50μm-150μm,烧结后的陶瓷颗粒被金属镍牢固包覆。
傳統陶瓷塗層在質量、能耗、以及環保等方麵都存在一定的問題,針對這一現象,提齣瞭預滲入法製備陶瓷塗層技術。即預先在坯體錶麵造齣孔洞,將陶瓷複閤粉料預先滲入到坯體錶麵的孔洞中,通過燒結,在金屬錶麵製備一層具有優異耐磨性的襯瓷層。研究瞭造孔劑加入量、預燒工藝等參數對孔分佈的影響規律,利用掃描電鏡分析瞭預燒後坯體的孔洞分佈規律和燒結後襯瓷層的顯微組織,實驗結果錶明:造孔劑的加入量(澱粉)為10%、預燒工藝參數為400℃×1h時,坯體中孔的分佈較為均勻,孔徑大小適閤納米氧化鋯的預滲入;預滲入法穫得的襯瓷層厚度為50μm-150μm,燒結後的陶瓷顆粒被金屬鎳牢固包覆。
전통도자도층재질량、능모、이급배보등방면도존재일정적문제,침대저일현상,제출료예삼입법제비도자도층기술。즉예선재배체표면조출공동,장도자복합분료예선삼입도배체표면적공동중,통과소결,재금속표면제비일층구유우이내마성적츤자층。연구료조공제가입량、예소공예등삼수대공분포적영향규률,이용소묘전경분석료예소후배체적공동분포규률화소결후츤자층적현미조직,실험결과표명:조공제적가입량(정분)위10%、예소공예삼수위400℃×1h시,배체중공적분포교위균균,공경대소괄합납미양화고적예삼입;예삼입법획득적츤자층후도위50μm-150μm,소결후적도자과립피금속얼뢰고포복。
Arming at the problems of ceramic - coating made in the traditional method in quality, energy consumption, and environmental protection, the new technology lining - ceramic - layer in surface of metal calling prepermeating technique is puts forward into. Namely some holes would be pre -prepared in the surface of the green body, and the ceramic composite powder infiltrated into the hole, and then lining ceram- ic layer which has excellent wear - resistance have formed in the metal surface by sintering. It was studied that influence rule of two factor both the addition amount of the starch and pre - burn process parameters to distribution of the holes, analyzed the distribution state of hole on the surface of green body and microstructure of lining - ceramic - layer using SEM. Result show that hole distribution uniform in the green body, and its size suits for permeating of granule of zirconia under such experiment condition that starch contents for 10% , pre - burn temperature at 400℃ × 1 hour; the thick of lining ceramic layer is 50μm - 150μm, ceramic particle was coated by nickel metal after sintering.