CAJ | 학술논문

采用顶空气相色谱-质谱联用(HS-GC/MS)法测定烟草行业标准YC263-2008卷烟条与包装纸中挥发性有机物溶剂残留,根据物质峰面积和标样浓度,计算回归方程,以及16种溶剂的线性范围、回收率、检出限、精密度等.通过胶粘剂、纸品样的实际检测,验证了方法的可行性,有效避免顶空气相色谱法的干扰问题,顶空气质联用法能准确地检测残留气体.
채용정공기상색보-질보련용(HS-GC/MS)법측정연초행업표준YC263-2008권연조여포장지중휘발성유궤물용제잔류,근거물질봉면적화표양농도,계산회귀방정,이급16충용제적선성범위、회수솔、검출한、정밀도등.통과효점제、지품양적실제검측,험증료방법적가행성,유효피면정공기상색보법적간우문제,정공기질련용법능준학지검측잔류기체.
Total of 16 volatile organic residual solvent compounds in the cigarette paper and the wrapping paper listed in standard YC263-2008 were analyzed by headspace gas chromatography-mass spectrometry(HS-GC/MS). The linear range, recovery rate, precision and detection limit of the 16 residual solvents were tested. The method proved to be successful by the testing results of the adhesive and wrapping paper samples, which can avoid the disturbance problem brought by HS-GC. The results show that HS-GC/MS tests the residual solvents effectively, and the veracity of HS-GC/MS is better than HS-GC.