化学工程师
化學工程師
화학공정사
CHEMICAL ENGINEER
2009年
7期
23-24
,共2页
张鑫%侯雪梅%闫丽%李传碧
張鑫%侯雪梅%閆麗%李傳碧
장흠%후설매%염려%리전벽
乙酰二茂铁%Schiff碱%呋喃甲酸%酰肼
乙酰二茂鐵%Schiff堿%呋喃甲痠%酰肼
을선이무철%Schiff감%부남갑산%선정
acetylferrocene%Schiff base%(a-)furancarboxylic acid%acyl hydrazide
本文由呋喃甲酸经酯化、酰肼化反应得到呋喃甲酸酰肼,再由乙酰二茂铁与呋喃甲酸酰肼在乙醇溶剂中反应得到含二茂铁基的呋喃甲酸酰腙,以红外光谱、核磁共振谱对产品进行确定.
本文由呋喃甲痠經酯化、酰肼化反應得到呋喃甲痠酰肼,再由乙酰二茂鐵與呋喃甲痠酰肼在乙醇溶劑中反應得到含二茂鐵基的呋喃甲痠酰腙,以紅外光譜、覈磁共振譜對產品進行確定.
본문유부남갑산경지화、선정화반응득도부남갑산선정,재유을선이무철여부남갑산선정재을순용제중반응득도함이무철기적부남갑산선종,이홍외광보、핵자공진보대산품진행학정.
In this paper, we used (a-)furancarboxylic acid as raw material, the compound of furan-2-caraoxylic acid hydrazide was synthesized by the ester spending reaction. The acyl hydrazine spending reaction;acetylferrocene reacted with furan-2-caraoxylic acid hydrazide in ethanol to give the compound containing ferrocenyl Schiff base furan-2-caraoxylic acid acyi hydrazone, the compound was determined by IR and 1HNMR spectrometer.
