CAJ | 학술논문

为研究定心藤中总有机酸的最佳提取工艺,建立其测定方法,采用正交实验法考察了乙醇含量、固液比、提取时间及提取次数4个因素对该工艺的影响, 利用电位滴定法对其进行了测定.结果表明,定心藤中总有机酸提取的最佳提取工艺为:乙醇含量75%,固液比1: 10,提取时间2.5 h,提取次数3次;电位滴定法对其测定简单可行,精密度高,重现性好,为定心藤进一步研究和资源开发利用提供一定的科学依据.
위연구정심등중총유궤산적최가제취공예,건립기측정방법,채용정교실험법고찰료을순함량、고액비、제취시간급제취차수4개인소대해공예적영향, 이용전위적정법대기진행료측정.결과표명,정심등중총유궤산제취적최가제취공예위:을순함량75%,고액비1: 10,제취시간2.5 h,제취차수3차;전위적정법대기측정간단가행,정밀도고,중현성호,위정심등진일보연구화자원개발이용제공일정적과학의거.
To study the optimum extracting process of total organic acids from Mappianthus iodoies and establish a determination method for total organic acid, the effects of concentration of ethanol, ratio of solid to liquid,frequency of extraction and time of extraction were investigated by orthogonal design and was determined with potential titration.The results show that the best extraction conditions are to use φ=75% ethanol as extractor with the radio of 1: 10 at the temperature of 80 ℃ for 2.5 h, and extracting 3 times.The determination method is simple, reproducible and suitable.It concludes these results provided certain scientific basis for further efficacy of research and development of Mappianthus iodoies.