中国动物保健
中國動物保健
중국동물보건
CHINA ANIMAL HEALTH
2012年
1期
15-17
,共3页
胡延春%赵春蕊%叶玉辉%叶卫列
鬍延春%趙春蕊%葉玉輝%葉衛列
호연춘%조춘예%협옥휘%협위렬
一针肥注射液%微量元素%测定方法
一針肥註射液%微量元素%測定方法
일침비주사액%미량원소%측정방법
YIZHENFEI injection%trace elements%assay method
目的:建立"一针肥注射液"中微量元素的含量测定方法。方法:采用火焰原子吸收分光光度法测定"一针肥注射液"中铁、锌、铜、硒、钴的含量。结果:铁、锌、铜、硒、钴的线性范围分别为0.053~0.385μg/mL、0.25~2.50μg/mL、0.5~8.0μg/mL、10.0~100.0ng/mL、5.0~50.0ng/mL,平均回收率分别为100.35%、99.95%、99.51%、98.49%、100.51%。结论:本法可以准确测定"一针肥注射液"中铁、锌、铜、硒、钴的含量,该法简便、快速、准确可靠。
目的:建立"一針肥註射液"中微量元素的含量測定方法。方法:採用火燄原子吸收分光光度法測定"一針肥註射液"中鐵、鋅、銅、硒、鈷的含量。結果:鐵、鋅、銅、硒、鈷的線性範圍分彆為0.053~0.385μg/mL、0.25~2.50μg/mL、0.5~8.0μg/mL、10.0~100.0ng/mL、5.0~50.0ng/mL,平均迴收率分彆為100.35%、99.95%、99.51%、98.49%、100.51%。結論:本法可以準確測定"一針肥註射液"中鐵、鋅、銅、硒、鈷的含量,該法簡便、快速、準確可靠。
목적:건립"일침비주사액"중미량원소적함량측정방법。방법:채용화염원자흡수분광광도법측정"일침비주사액"중철、자、동、서、고적함량。결과:철、자、동、서、고적선성범위분별위0.053~0.385μg/mL、0.25~2.50μg/mL、0.5~8.0μg/mL、10.0~100.0ng/mL、5.0~50.0ng/mL,평균회수솔분별위100.35%、99.95%、99.51%、98.49%、100.51%。결론:본법가이준학측정"일침비주사액"중철、자、동、서、고적함량,해법간편、쾌속、준학가고。
The purpose of this paper is to construct the assay method of trace elements from YIZHENFEI injection. The content of Fe, Zn, Cu, Se, Co element was measured by Flame atomic absorption spectrophotometric (AAS) method. The results showed that linear range of Fe, Zn, Cu, Se, Co from YIZHENFEI injection were 0.053~0.385μg/mL, 0.25~2.50μg/mL, 0.5~8.0μg/mL, 10.0~100.0 ng/mL and 5.0~50.0 ng/mL, respectively. And their average recoveries were 100.35%, 99.95%, 99.51%, 98.49% and 100.51%, respectively. In conclusion, Flame ASS method can measure the content of Fe, Zn, Cu, Se, Co element from YIZHENFEI injection accurately, quickly and conveniently.