玉溪师范学院学报
玉溪師範學院學報
옥계사범학원학보
JOURNAL OF YUXI TEACHERS COLLEGE
2011年
8期
36-40
,共5页
闫辉%李枝武%吴文锐%倪明
閆輝%李枝武%吳文銳%倪明
염휘%리지무%오문예%예명
甲氰菊酯%小白菜%土壤%残留%消解
甲氰菊酯%小白菜%土壤%殘留%消解
갑청국지%소백채%토양%잔류%소해
fenpropathrin%cabbage%soil%residue%digestion
为评价杀虫剂甲氰菊酯在小白菜上使用后的残留行为及环境安全性,采用乙腈提取白菜和土壤中残留的甲氰菊酯,经Florisil柱层析净化后,用GC/ECD方法对甲氰菊酯在白菜和土壤中的残留进行了研究.实验结果表明:甲氰菊酯在小白菜和土壤中的降解半衰期分别为3 d和14 d,在推荐使用剂量下,在白菜上施药14d后残留量低于我国规定的最大残留限量0.5 mg.kg-1,21 d后残留量低于日本规定的最大残留限量0.1 mg.kg-1.
為評價殺蟲劑甲氰菊酯在小白菜上使用後的殘留行為及環境安全性,採用乙腈提取白菜和土壤中殘留的甲氰菊酯,經Florisil柱層析淨化後,用GC/ECD方法對甲氰菊酯在白菜和土壤中的殘留進行瞭研究.實驗結果錶明:甲氰菊酯在小白菜和土壤中的降解半衰期分彆為3 d和14 d,在推薦使用劑量下,在白菜上施藥14d後殘留量低于我國規定的最大殘留限量0.5 mg.kg-1,21 d後殘留量低于日本規定的最大殘留限量0.1 mg.kg-1.
위평개살충제갑청국지재소백채상사용후적잔류행위급배경안전성,채용을정제취백채화토양중잔류적갑청국지,경Florisil주층석정화후,용GC/ECD방법대갑청국지재백채화토양중적잔류진행료연구.실험결과표명:갑청국지재소백채화토양중적강해반쇠기분별위3 d화14 d,재추천사용제량하,재백채상시약14d후잔류량저우아국규정적최대잔류한량0.5 mg.kg-1,21 d후잔류량저우일본규정적최대잔류한량0.1 mg.kg-1.
To evaluate the residue variation and environment security of using fenpropathrin in cabbage,fenpropathrin residue in cabbage and soil samples were extracted with acetonitrile,cleaned up by a column of Florisil,and detected by means of GC/ECD.The results indicated that the half-life of fenpropathrin in cabbage and soil were 3days and 14days;after fenpropathrin was used at the recommended dosage 14 days,the residues in cabbage were below the MRL1.0mg.kg set in China;after 21 days,the residues in cabbage were below the MRL 0.5mg.kg-1 set by Japan.