无锡轻工大学学报
無錫輕工大學學報
무석경공대학학보
JOURNAL OF WUXI UNIVERSITY OF LIGHT INDUSTRY
2001年
2期
214-216
,共3页
戴军%王彬%倪永全
戴軍%王彬%倪永全
대군%왕빈%예영전
高效液相色谱法%聚甘油%保留值%分析方法
高效液相色譜法%聚甘油%保留值%分析方法
고효액상색보법%취감유%보류치%분석방법
采用HPLC分析了聚甘油的组成,其线性聚甘油及环状聚甘油的保留时间的对数均与其相对分子质量呈线性正相关,线性方程分别为lg tR=0.0013 M+2.5047和lg tR=0.0018 M+2.3220.用化学法和HPLC两种方法测定聚甘油样品中甘油的含量,结果基本一致.
採用HPLC分析瞭聚甘油的組成,其線性聚甘油及環狀聚甘油的保留時間的對數均與其相對分子質量呈線性正相關,線性方程分彆為lg tR=0.0013 M+2.5047和lg tR=0.0018 M+2.3220.用化學法和HPLC兩種方法測定聚甘油樣品中甘油的含量,結果基本一緻.
채용HPLC분석료취감유적조성,기선성취감유급배상취감유적보류시간적대수균여기상대분자질량정선성정상관,선성방정분별위lg tR=0.0013 M+2.5047화lg tR=0.0018 M+2.3220.용화학법화HPLC량충방법측정취감유양품중감유적함량,결과기본일치.
The compositions of the polyglycerols were analyzed by HPLC on the YWGNH2 Column in this paper. Each logarithm of retention time (tR) of the linear polyglycerol and the cyclic polyglycerol v.s. its molecular weight is linear correlative. The linear equation is lg tR=0.0013 M+2.5047 and lg tR=0.0018 M+2.3220 respectively. The contents of the glycerol in the polyglycerols determined by the chemical method and HPLC were compared.