2,4-二硝基溴苯的合成
2,4-이초기추분적합성
Synthesis of 1-bromo-2,4-dinitrobenzene
  • 万方数据
    化学试剂 화학시제
    CHEMICAL REAGENTS
    2010年 2期 181-182 ,共2页

    吉轩%韩艳辉%张鑫%魏红玉%张昭

    길헌%한염휘%장흠%위홍옥%장소

    溴苯%2%4-二硝基溴苯%硝化反应 溴苯%2%4-二硝基溴苯%硝化反應
    추분%2%4-이초기추분%초화반응
    bromobenzene%1-bromo-2%4-dinitrobenzene%nitration
    以溴苯为原料,在水中与硝酸、硫酸混合酸反应合成了标题化合物,产率94.8%,纯度质量分数高于99.0%.所得产物的结构通过了红外、核磁波谱的表征.
    이추분위원료,재수중여초산、류산혼합산반응합성료표제화합물,산솔94.8%,순도질량분수고우99.0%.소득산물적결구통과료홍외、핵자파보적표정.
    1-Bromo-2,4-dinitrobenzene,used as the intermediate of medicinal and pharmaceutical agents,organic dyes,organic electroluminescent material,was synthesized from bromobenzene by nitration in water.The yield of 1-bromo-2,4-dinitrobenzene reached 94.8% and the product purity was higher than 99.0%.The structure of target product was characterized by IR and NMR spectrometry.
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