分析测试学报
分析測試學報
분석측시학보
JOURNAL OF INSTRUMENTAL ANALYSIS
2001年
1期
55-57
,共3页
微波消解%氢化物发生%电感耦合等离子体发射光谱%化妆品%汞%砷%铅
微波消解%氫化物髮生%電感耦閤等離子體髮射光譜%化妝品%汞%砷%鉛
미파소해%경화물발생%전감우합등리자체발사광보%화장품%홍%신%연
采用微波消解－氢化物发生ICP－AES法测定化妆品中的Hg、As和Pb，加入L-半胱氨酸消除了过渡金属离子的干扰，考察了微波消解、氢化物发生的最佳条件。建立的方法简便快速，测定Hg、As和Pb的RSD分别为0.59％、1.2％、2.4％（n=10），样品加标回收率分别为98.5％、99.3％和100.1％。该法已应用于化妆品的常规测定，得到满意的结果。
採用微波消解－氫化物髮生ICP－AES法測定化妝品中的Hg、As和Pb，加入L-半胱氨痠消除瞭過渡金屬離子的榦擾，攷察瞭微波消解、氫化物髮生的最佳條件。建立的方法簡便快速，測定Hg、As和Pb的RSD分彆為0.59％、1.2％、2.4％（n=10），樣品加標迴收率分彆為98.5％、99.3％和100.1％。該法已應用于化妝品的常規測定，得到滿意的結果。
채용미파소해－경화물발생ICP－AES법측정화장품중적Hg、As화Pb，가입L-반광안산소제료과도금속리자적간우，고찰료미파소해、경화물발생적최가조건。건립적방법간편쾌속，측정Hg、As화Pb적RSD분별위0.59％、1.2％、2.4％（n=10），양품가표회수솔분별위98.5％、99.3％화100.1％。해법이응용우화장품적상규측정，득도만의적결과。
A microwave assisted digestion－hydride generation ICP－AES methodwas established for the determination of Hg， As and Pb in cosmetics. The experimental conditions of microwave assisted digestion－hydride generation were optimized. The interference of transitional elements in cosmetics was eliminated by the addition of an appropriate amount of L-cysteine. The recoveries of the method for Hg, As and Pb of standard samples were found to be 98.5％ , 100.1％ , 99.3％ , respectively, while RSD(n=10) is 0.59％ for Hg,1.2％ for As and 2.4％ for Pb. The method has been applied to the analysis of cosmetics with satisfactory results.
