浙江大学学报(英文版)
浙江大學學報(英文版)
절강대학학보(영문판)
JOURNAL OF ZHEJIANG UNIVERSITY SCIENCE
2004年
8期
956-959
,共4页
文岳中%方兆华%刘维屏
文嶽中%方兆華%劉維屏
문악중%방조화%류유병
Cleaner preparation,Greener technology,Selective synthesis,2-methyl-benzene-l,3-diol,3-(4,6-dimeth-oxy-pyrimidin-2-yloxy)-2-methyl-phenol
Environmental concerns have highlighted the need of cleaner technologies. A cleaner, convenient and selectivetechnology has been developed for the preparation of 3-(4,6-dimethoxy-pyrimidin-2-yloxy)-2-methyl-phenol (DPMP) from2-methyl-benzene-l,3-diol in water as solvent. The isolated yield of DPMP is up to 86% in good selectivity. The productstructure was characterized by conventional methods, 1H-NMR and MS. This technology belongs to the modern concept ofenvironmentally friendly low wastes or non-wastes technology (LWNWT).
