西安建筑科技大学学报(自然科学版)
西安建築科技大學學報(自然科學版)
서안건축과기대학학보(자연과학판)
JOURNAL OF XI'AN UNIVERSITY OF ARCHITECTURE & TECHNOLOGY
2005年
3期
411-415
,共5页
肖国庆%高志鹏%荆桂花%庞锐
肖國慶%高誌鵬%荊桂花%龐銳
초국경%고지붕%형계화%방예
magnesium aluminate spinel%cement%dolomite%additive
以白云石和工业三氧化二铝为原料,采用反应烧结技术制得了含镁铝尖晶石的铝酸盐水泥,探讨了原料及烧结温度和添加剂对含镁铝尖晶石的铝酸盐水泥性能的影响,XRD结果表明产物的物相组成为MA,CA,CA2;采用扫描电镜(SEM)及能谱(EDS)对产物的显微结构进行了观察与分析.结果表明:以轻烧白云石和工业Al2O3为原料制得的水泥具有较高的结合强度;所制得的含镁铝尖晶石的铝酸盐水泥的显微结构较为均匀,外加剂CaCl2具有明显的早强效果.
以白雲石和工業三氧化二鋁為原料,採用反應燒結技術製得瞭含鎂鋁尖晶石的鋁痠鹽水泥,探討瞭原料及燒結溫度和添加劑對含鎂鋁尖晶石的鋁痠鹽水泥性能的影響,XRD結果錶明產物的物相組成為MA,CA,CA2;採用掃描電鏡(SEM)及能譜(EDS)對產物的顯微結構進行瞭觀察與分析.結果錶明:以輕燒白雲石和工業Al2O3為原料製得的水泥具有較高的結閤彊度;所製得的含鎂鋁尖晶石的鋁痠鹽水泥的顯微結構較為均勻,外加劑CaCl2具有明顯的早彊效果.
이백운석화공업삼양화이려위원료,채용반응소결기술제득료함미려첨정석적려산염수니,탐토료원료급소결온도화첨가제대함미려첨정석적려산염수니성능적영향,XRD결과표명산물적물상조성위MA,CA,CA2;채용소묘전경(SEM)급능보(EDS)대산물적현미결구진행료관찰여분석.결과표명:이경소백운석화공업Al2O3위원료제득적수니구유교고적결합강도;소제득적함미려첨정석적려산염수니적현미결구교위균균,외가제CaCl2구유명현적조강효과.
A new type of calcium aluminate cement containing MA spinel was produced by sintering the raw materials of dolomite and alumina mixture. The effects of raw materials and sintering temperature and additives on the properties of cements was were investigated. X-ray diffraction (XRD) results indicate that the final products consisted of CA, CA2and MA. The microstructure of product was analyzed by means of scanning electron microscope (SEM)and energy dispersive spectrometry (EDS). The experiments results showed that the cement had the satisfied cold bonding strength and sintering properties when the light-burned dolomite and alumina were employed and fired at 1600C. The new type cements has relatively uniform microstructure The early stage strength of the refractory castables bodies was greatly improved by adding 2wt. % of CaCl2 as a strength modifier.