CAJ | 학술논문

目的：从兰科植物流苏石斛（Dendrobium fimbriatum Hook.）茎中提取分离活性成分。方法：95%乙醇提取、溶剂抽提、硅胶柱层析、重结晶等。结果：分离出9个化合物，鉴定出其中6个，分别为大黄酚（3）、三十二烷酸（5）、对羟基反式肉桂酸三十烷基酯（6）、对羟基顺式肉桂酸三十烷基酯（7）、β-谷甾醇（8）和鼓槌联苄（9）。结论：大黄酚为首次从石斛属植物中分得，鼓槌联苄为首次从该种植物中分离得到。
목적：종란과식물류소석곡（Dendrobium fimbriatum Hook.）경중제취분리활성성분。방법：95%을순제취、용제추제、규효주층석、중결정등。결과：분리출9개화합물，감정출기중6개，분별위대황분（3）、삼십이완산（5）、대간기반식육계산삼십완기지（6）、대간기순식육계산삼십완기지（7）、β-곡치순（8）화고퇴련변（9）。결론：대황분위수차종석곡속식물중분득，고퇴련변위수차종해충식물중분리득도。
AIM　Bio-active constituents were expected to be obtained from Dendrobium fimbriatum Hook. METHODS　It was extracted with 95% alcohol, distributed by petrol, isolated via column chromatography on silica gel and purified by crystallization. RESULTS　Nine compounds were isolated from the stems of Dendrobium fimbriatum Hook., On the basis of spectral analyses, six compounds of them were identified as chrysophanol(3), n-dotriacodtanoic acid(5), defuscin(6), n-triacontyl cis-p-coumarate(7), β-sitosterol(8) and chrysotobibenzyl(9). CONCLUSION　Chrysophanol(3) was firstly isolated from Genus dendrobium and chrysotobibenzyl(9) was found from this species for the first time.