广州化工
廣州化工
엄주화공
GUANGZHOU CHEMICAL INDUSTRY AND TECHNOLOGY
2012年
1期
40-42
,共3页
液相化学还原法%油溶性%纳米铜
液相化學還原法%油溶性%納米銅
액상화학환원법%유용성%납미동
liquid phase chemical synthesis%oil-solubility%nano-Cu
采用液相化学还原法,以硫酸铜为原料,抗坏血酸作还原剂,吐温-80作修饰剂,用正交实验方法获得了油溶性纳米铜的最佳的合成条件：抗坏血酸为3 g,吐温-80为30 mL,正丁醇为70 mL,反应温度95℃。并利用X射线衍射仪对产品进行表征测试。
採用液相化學還原法,以硫痠銅為原料,抗壞血痠作還原劑,吐溫-80作脩飾劑,用正交實驗方法穫得瞭油溶性納米銅的最佳的閤成條件：抗壞血痠為3 g,吐溫-80為30 mL,正丁醇為70 mL,反應溫度95℃。併利用X射線衍射儀對產品進行錶徵測試。
채용액상화학환원법,이류산동위원료,항배혈산작환원제,토온-80작수식제,용정교실험방법획득료유용성납미동적최가적합성조건：항배혈산위3 g,토온-80위30 mL,정정순위70 mL,반응온도95℃。병이용X사선연사의대산품진행표정측시。
The optimal synthesis conditions of the oil soluble nanometer copper were obtained by orthogonal experiment method,under the conditions of copper sulfate as raw material,3 g ascorbic acid as reducing agent,and 30 mL Tween-80 as modifiers,70 mL n-butanol as solution,and reaction temperature 95 ℃.The product was characterized using X-ray diffraction.
