大学物理实验
大學物理實驗
대학물리실험
PHYSICAL EXPERIMENT OF COLLEGE
2011年
5期
18-20
,共3页
谢娟%高晓蕊%谢艳%孟晓彩%边丽
謝娟%高曉蕊%謝豔%孟曉綵%邊麗
사연%고효예%사염%맹효채%변려
物理分析技术%ZnO%形貌%晶体结构
物理分析技術%ZnO%形貌%晶體結構
물리분석기술%ZnO%형모%정체결구
physics analysis technique%ZnO%morphology%crystal structure
以氯化锌和氢氧化钠为主要原料,采用简单液相法,通过改变反应液的组成,制备出了针状、棒状、片状和花状四种不同形貌的ZnO微/纳米晶体。应用X-射线粉末衍射仪(XRD),扫描电子显微镜(SEM)、高分辨透射电子显微镜(HRTEM)及选区电子衍射仪(SEAD)对产物进行表征,获得了ZnO物相、形貌与微观结构的重要信息。
以氯化鋅和氫氧化鈉為主要原料,採用簡單液相法,通過改變反應液的組成,製備齣瞭針狀、棒狀、片狀和花狀四種不同形貌的ZnO微/納米晶體。應用X-射線粉末衍射儀(XRD),掃描電子顯微鏡(SEM)、高分辨透射電子顯微鏡(HRTEM)及選區電子衍射儀(SEAD)對產物進行錶徵,穫得瞭ZnO物相、形貌與微觀結構的重要信息。
이록화자화경양화납위주요원료,채용간단액상법,통과개변반응액적조성,제비출료침상、봉상、편상화화상사충불동형모적ZnO미/납미정체。응용X-사선분말연사의(XRD),소묘전자현미경(SEM)、고분변투사전자현미경(HRTEM)급선구전자연사의(SEAD)대산물진행표정,획득료ZnO물상、형모여미관결구적중요신식。
Using zinc chloride and sodium hydroxide as the main reactants,needle-,rod-,plate-,and flower-like ZnO micro-/nanocrystals were successfully prepared via a low-temperature liquid phase method,by controlling the composition of precursor solution.X-ray diffraction(XRD),scanning electron microscopy(SEM),high resolution transmission electron microscope(HRTEM) and selected area electron diffraction(SAED) were used to characterize the products.Some important information of ZnO crystal was obtained,such as phase,morphology and microstructure.