稀有金属材料与工程
稀有金屬材料與工程
희유금속재료여공정
RARE METAL MATERIALS AND ENGINEERNG
2011年
3期
377-383
,共7页
郭强%王清%韩秀丽%鲁学锟%孙东立%武高辉
郭彊%王清%韓秀麗%魯學錕%孫東立%武高輝
곽강%왕청%한수려%로학곤%손동립%무고휘
β钛合金%时效%α析出相%显微硬度%力学性能
β鈦閤金%時效%α析齣相%顯微硬度%力學性能
β태합금%시효%α석출상%현미경도%역학성능
β-titanium alloy%aging%α precipitate%microhardness%mechanical properties
研究了大变形量冷轧Ti-15-3合金的时效析出行为和时效过程中力学性能的变化.冷变形使Ti-15-3合金中形成部分纳米晶.冷变形合金在450~650℃时效时,从β相纳米晶区析出极为细小的针状α相,而从β相非纳米晶区析出的α相随着时效温度的升高由针状逐渐长大为条状,进而演变为凸透镜状.冷变形合金在450℃时效4 h后,硬度达到了峰值,HV为5328 MPa.450℃时效时在硬度峰值处同样达到了强度峰值,屈服强度和抗拉强度分别可高达1483和1562 MPa.时效温度升高,达到峰值硬度的时间缩短,硬度值大幅度下降.650℃时效后的强度和硬度均低于时效前,粗大的透镜状析出相、纳米晶的长大以及位错密度的急剧下降是650℃时效时硬化效果消失的主要原因.不同时效工艺下的强度和硬度的变化规律相似,性能的变化与时效过程中析出相的状态有关.
研究瞭大變形量冷軋Ti-15-3閤金的時效析齣行為和時效過程中力學性能的變化.冷變形使Ti-15-3閤金中形成部分納米晶.冷變形閤金在450~650℃時效時,從β相納米晶區析齣極為細小的針狀α相,而從β相非納米晶區析齣的α相隨著時效溫度的升高由針狀逐漸長大為條狀,進而縯變為凸透鏡狀.冷變形閤金在450℃時效4 h後,硬度達到瞭峰值,HV為5328 MPa.450℃時效時在硬度峰值處同樣達到瞭彊度峰值,屈服彊度和抗拉彊度分彆可高達1483和1562 MPa.時效溫度升高,達到峰值硬度的時間縮短,硬度值大幅度下降.650℃時效後的彊度和硬度均低于時效前,粗大的透鏡狀析齣相、納米晶的長大以及位錯密度的急劇下降是650℃時效時硬化效果消失的主要原因.不同時效工藝下的彊度和硬度的變化規律相似,性能的變化與時效過程中析齣相的狀態有關.
연구료대변형량랭알Ti-15-3합금적시효석출행위화시효과정중역학성능적변화.랭변형사Ti-15-3합금중형성부분납미정.랭변형합금재450~650℃시효시,종β상납미정구석출겁위세소적침상α상,이종β상비납미정구석출적α상수착시효온도적승고유침상축점장대위조상,진이연변위철투경상.랭변형합금재450℃시효4 h후,경도체도료봉치,HV위5328 MPa.450℃시효시재경도봉치처동양체도료강도봉치,굴복강도화항랍강도분별가고체1483화1562 MPa.시효온도승고,체도봉치경도적시간축단,경도치대폭도하강.650℃시효후적강도화경도균저우시효전,조대적투경상석출상、납미정적장대이급위착밀도적급극하강시650℃시효시경화효과소실적주요원인.불동시효공예하적강도화경도적변화규률상사,성능적변화여시효과정중석출상적상태유관.
The precipitation behavior of α phase from β phase and the variation of mechanical properties during aging in the severely cold rolled alloy were studied. The results show that nanostructure is formed in some regions of the cold deformed alloy, α phases precipitating from β nanostructure region are thin-needle like during aging from 450 ℃ to 650 ℃ and those from β non-nanostructure region grow from the needle to the lath-shaped and finally become lenticular plate. After cold rolling and heat treatment at 450 ~C for 4 h, the hardness of the alloy reaches the peak value (5328 MPa). The yield strength and ultimate strength of the alloy aged at 450℃ for 4 h are 1483 and 1562 MPa, respectively. The aging time for peak value is shortened and the hardness decreases sharply with the increase of aging temperature. The strength and hardness of the alloy after aging at 650 ℃ is lower than that before aging. This is attributed to the coarse thin-plate precipitates, the growth of nanostructure crystals and the decrease of dislocation density in the alloy during aging at 650 ℃. The change tendency of the strength and the hardness of the alloy treated by different aging procedures are similar and they are related to the state of the precipitates formed during aging.