鞍山师范学院学报
鞍山師範學院學報
안산사범학원학보
JOURNAL OF ANSHAN TEACHERS COLLEGE
2011年
6期
26-29
,共4页
回瑞华%侯冬岩%李铁纯%丛秀枝%吴祎林
迴瑞華%侯鼕巖%李鐵純%叢秀枝%吳祎林
회서화%후동암%리철순%총수지%오의림
烟草%尼古丁%气相色谱-质谱法%同时蒸馏萃取%水蒸气蒸馏
煙草%尼古丁%氣相色譜-質譜法%同時蒸餾萃取%水蒸氣蒸餾
연초%니고정%기상색보-질보법%동시증류췌취%수증기증류
Tobacco%Nicotine%Gas chromatography/Mass spectrometry%Simultaneous distillation extraction%Water distillation extraction
采用同时蒸馏萃取法与水蒸气蒸馏法提取烟草中挥发性成分并用气相色谱-质谱(GC/MS)法分别确认其化学成分,其中主要成分为尼古丁.用气相色谱法测定烟草中尼古丁的含量.尼古丁含量在0.446 4~0.892 8 mg/mL范围内与峰面积呈良好线性关系,回归方程为:A=61 670 M-2 894.8,相关系数为0.998 6,回收率为99.83%.
採用同時蒸餾萃取法與水蒸氣蒸餾法提取煙草中揮髮性成分併用氣相色譜-質譜(GC/MS)法分彆確認其化學成分,其中主要成分為尼古丁.用氣相色譜法測定煙草中尼古丁的含量.尼古丁含量在0.446 4~0.892 8 mg/mL範圍內與峰麵積呈良好線性關繫,迴歸方程為:A=61 670 M-2 894.8,相關繫數為0.998 6,迴收率為99.83%.
채용동시증류췌취법여수증기증류법제취연초중휘발성성분병용기상색보-질보(GC/MS)법분별학인기화학성분,기중주요성분위니고정.용기상색보법측정연초중니고정적함량.니고정함량재0.446 4~0.892 8 mg/mL범위내여봉면적정량호선성관계,회귀방정위:A=61 670 M-2 894.8,상관계수위0.998 6,회수솔위99.83%.
Simultaneous distillation extraction method(SDE) and water distillation extraction method(WDE) are used for extracting the volatile chemical constituents of tobaccos and the chemical components are identified by gas chromatography/mass spectrometry(GC/MS) method respectively.Of them the major compound is nicotine.The contents of nicotine in tobaccos are determinated by gas chromatographic method.A good linear relationship between the concentrations in 0.446 4~0.892 8 mg/mL with peak area is found.The regression equation is A=61 670M-2 894.8 and correlation coefficient 0.998 6,the average recovery of the method is 99.83%.