酿酒科技
釀酒科技
양주과기
LIQUOR-MAKING SCIENCE & TECHNOLOGY
2011年
9期
71-73
,共3页
刘源才%胡辉%陈敬炳%陈洪莲%黄秀华%刘鑫%邹伟%冯声宝
劉源纔%鬍輝%陳敬炳%陳洪蓮%黃秀華%劉鑫%鄒偉%馮聲寶
류원재%호휘%진경병%진홍련%황수화%류흠%추위%풍성보
中国劲酒%挥发性风味物质%气相色谱-质谱%结构鉴定
中國勁酒%揮髮性風味物質%氣相色譜-質譜%結構鑒定
중국경주%휘발성풍미물질%기상색보-질보%결구감정
Jing wine%volatile flavoring substances%GC-MS%structural identification
采用溶剂法和水蒸汽蒸馏法提取中国劲酒的挥发性风味物质,用气相色谱一质谱联用法(GC—MS)对其化学组分进行分离及鉴定。结果表明,共定性出30种化学成分,其中挥发性风味物质中的主要识别成分及部分功能性微量成分为:乙酸龙脑酯、丁香酚及其异构体、十八碳二烯酸以及二十二碳六烯酸(DHA);丁香酚及其异构体占挥发性成分的4.85%(以峰面积计):有机溶剂提取与水蒸汽蒸馏相结合法可快速提取劲酒中的挥发性风味物质。
採用溶劑法和水蒸汽蒸餾法提取中國勁酒的揮髮性風味物質,用氣相色譜一質譜聯用法(GC—MS)對其化學組分進行分離及鑒定。結果錶明,共定性齣30種化學成分,其中揮髮性風味物質中的主要識彆成分及部分功能性微量成分為:乙痠龍腦酯、丁香酚及其異構體、十八碳二烯痠以及二十二碳六烯痠(DHA);丁香酚及其異構體佔揮髮性成分的4.85%(以峰麵積計):有機溶劑提取與水蒸汽蒸餾相結閤法可快速提取勁酒中的揮髮性風味物質。
채용용제법화수증기증류법제취중국경주적휘발성풍미물질,용기상색보일질보련용법(GC—MS)대기화학조분진행분리급감정。결과표명,공정성출30충화학성분,기중휘발성풍미물질중적주요식별성분급부분공능성미량성분위:을산용뇌지、정향분급기이구체、십팔탄이희산이급이십이탄륙희산(DHA);정향분급기이구체점휘발성성분적4.85%(이봉면적계):유궤용제제취여수증기증류상결합법가쾌속제취경주중적휘발성풍미물질。
The volatile flavoring substances of Jing wine were extraced by organic solvent method and steam distillation. GC-MS analysis was conducted to identify their chemical structures. The results indicated that there identified 30 kinds of chemcial compounds, the main flavoring substances and functional trace components included bormeol acetate, cugnol, 9,12-octadecadienoic acid, and 4,7,10,13,16,19- docosahexaenoicacid methylester (DHA), eugnol and eugnol isomer accounted for 4.85 % of the total content of volatile flavoring substances (counted by peak area), and the combination of organic solvent method and steam distillation could rapidly extract the volatile flavoring substances of Jing wine.