聊城大学学报:自然科学版
聊城大學學報:自然科學版
료성대학학보:자연과학판
Journal of Liaocheng University:Natural Science Edition
2011年
2期
50-52,56
,共4页
刘燕燕%臧国忠%郭晴%王燕
劉燕燕%臧國忠%郭晴%王燕
류연연%장국충%곽청%왕연
无铅压电陶瓷%KNN%温度稳定性%压电常数
無鉛壓電陶瓷%KNN%溫度穩定性%壓電常數
무연압전도자%KNN%온도은정성%압전상수
Lead-free piezoelectric ceramics%KNN%thermal stability%piezoelectric constant
采用传统的固相反应法和普通的烧结工艺,分别制备了(Ko.48Nao.52)1-χ。(LiSb)χNb1-O3(χ=0.055,0.060,0.065)和χ=0.055,0=0.065按摩尔比1:1复合的无铅压电陶瓷样品(55-65),并对样品的压电、介电等性能进行了测试研究.实验结果表明:55-65不等同于χ=0.060的组分,其压电性能远低于χ=0.060的样品,进一步研究表明,相同烧结温度下,55-65样品的损耗较高,晶粒难以生长,相对较小,较小的晶粒可能在样品形变时产生的应力较大,这可能是55—65样品压电性能较低的原因.
採用傳統的固相反應法和普通的燒結工藝,分彆製備瞭(Ko.48Nao.52)1-χ。(LiSb)χNb1-O3(χ=0.055,0.060,0.065)和χ=0.055,0=0.065按摩爾比1:1複閤的無鉛壓電陶瓷樣品(55-65),併對樣品的壓電、介電等性能進行瞭測試研究.實驗結果錶明:55-65不等同于χ=0.060的組分,其壓電性能遠低于χ=0.060的樣品,進一步研究錶明,相同燒結溫度下,55-65樣品的損耗較高,晶粒難以生長,相對較小,較小的晶粒可能在樣品形變時產生的應力較大,這可能是55—65樣品壓電性能較低的原因.
채용전통적고상반응법화보통적소결공예,분별제비료(Ko.48Nao.52)1-χ。(LiSb)χNb1-O3(χ=0.055,0.060,0.065)화χ=0.055,0=0.065안마이비1:1복합적무연압전도자양품(55-65),병대양품적압전、개전등성능진행료측시연구.실험결과표명:55-65불등동우χ=0.060적조분,기압전성능원저우χ=0.060적양품,진일보연구표명,상동소결온도하,55-65양품적손모교고,정립난이생장,상대교소,교소적정립가능재양품형변시산생적응력교대,저가능시55—65양품압전성능교저적원인.
Lead-free Piezoelectric ceramics (K0.48Na0.52)l-χ(LiSb)xNbl-xO3 (x=0. 055,0. 060,0. 065), the composition compounded with x=0.055, x=0. 065 in mol ratio 1:1 (55-65) are fabricated by con- ventional solid-state sintering method, and the dielectric and piezoelectric characteristics are investiga- ted. It is found that the piezoelectric properties of 55-65 is much lower than that of the sample with x= 0. 060. Further investigations show that the sample 55-65 has relatively high dielectric loss and small grains. The smaller grains may lead to stronger stress with the same strain and this may be the reason for the sample 55-65 exhibiting low piezoelectric activities.