材料导报
材料導報
재료도보
MATERIALS REVIEW
2009年
z1期
159-160,163
,共3页
王尚平%徐华平%钟声亮%黄宜祥
王尚平%徐華平%鐘聲亮%黃宜祥
왕상평%서화평%종성량%황의상
纳米结构%纳米线%溶剂热%银
納米結構%納米線%溶劑熱%銀
납미결구%납미선%용제열%은
nanostructures%nanowire%solvothermal%silver
以聚乙烯吡咯烷酮(PVP)为表面活性剂、乙二醇为溶剂,通过简易的溶剂热方法合成了银纳米线.结果表明,在反应体系中乙二醇不仅能作为溶剂,而且还能起到还原剂的作用.用XRD、SEM对产物进行了表征.考察了乙二醇和PVP用量等对银纳米线合成的影响;找出了合成的较佳条件.对银纳米线的合成机理进行了初步探讨.
以聚乙烯吡咯烷酮(PVP)為錶麵活性劑、乙二醇為溶劑,通過簡易的溶劑熱方法閤成瞭銀納米線.結果錶明,在反應體繫中乙二醇不僅能作為溶劑,而且還能起到還原劑的作用.用XRD、SEM對產物進行瞭錶徵.攷察瞭乙二醇和PVP用量等對銀納米線閤成的影響;找齣瞭閤成的較佳條件.對銀納米線的閤成機理進行瞭初步探討.
이취을희필각완동(PVP)위표면활성제、을이순위용제,통과간역적용제열방법합성료은납미선.결과표명,재반응체계중을이순불부능작위용제,이차환능기도환원제적작용.용XRD、SEM대산물진행료표정.고찰료을이순화PVP용량등대은납미선합성적영향;조출료합성적교가조건.대은납미선적합성궤리진행료초보탐토.
Silver nanowires are prepared by a simple solvothermal reaction with ethylene glycol as solvent and poly N-vinylpyrrolidone(PVP) as surfactant.Results show that ethylene glycol not only serves as solvent but also reducing agent during the reaction.The products are characterized by XRD,SEM.The effects of the dosage of ethylene glycol and PVP on the preparation of silver nanowires are investigated in details.Results demonstrate that the dosage of ethylene glycol and PVP exert significant influence on the synthesis of silver nanowires.The optimal reaction conditions for the preparation ofthe silver nanowires are found.The possible formation mechanism for the silver nanowires is briefly discussed.