化学试剂
化學試劑
화학시제
CHEMICAL REAGENTS
2010年
3期
271-272
,共2页
光稳定剂%2,2′-硫代双对叔辛基苯酚%合成%晶体结构
光穩定劑%2,2′-硫代雙對叔辛基苯酚%閤成%晶體結構
광은정제%2,2′-류대쌍대숙신기분분%합성%정체결구
light stabilizer%2,2′-thiobis-4-tert-octylphenol%synthesis%crystal structure
合成了标题化合物.通过IR、1HNMR及X-射线单晶衍射对其结构进行了表征.该晶体属三斜晶系,P-1空间群,a=11.068(4) nm,b=11.226(5) nm,c=11.916(5) nm,α=83.004(7)°,β=75.641(7)°,V=1.337 8(9) nm3,Z=2,D_c=1.094 g/cm3,F(000)=480,R_1=0.064 3,wR_2=0.200 4.
閤成瞭標題化閤物.通過IR、1HNMR及X-射線單晶衍射對其結構進行瞭錶徵.該晶體屬三斜晶繫,P-1空間群,a=11.068(4) nm,b=11.226(5) nm,c=11.916(5) nm,α=83.004(7)°,β=75.641(7)°,V=1.337 8(9) nm3,Z=2,D_c=1.094 g/cm3,F(000)=480,R_1=0.064 3,wR_2=0.200 4.
합성료표제화합물.통과IR、1HNMR급X-사선단정연사대기결구진행료표정.해정체속삼사정계,P-1공간군,a=11.068(4) nm,b=11.226(5) nm,c=11.916(5) nm,α=83.004(7)°,β=75.641(7)°,V=1.337 8(9) nm3,Z=2,D_c=1.094 g/cm3,F(000)=480,R_1=0.064 3,wR_2=0.200 4.
The title compound had been synthesized and characterized by IR,1HNMR and single-crystal X-ray diffractometry.The test results showed that the crystal belonged to a triclinic system and the P-1 space group with following parameters:a=11.068(4) nm,b=11.226(5) nm,c=11.916(5) nm,and α=83.004(7)°,β=75.641(7)°,V=1.337 8(9) nm3,Z=2,D_c=1.094 g/cm3,F(000)=480,R_1=0.064 3,and wR_2=0.200 4.
