CAJ | 학술논문

目的：探讨速效消炎膏的定性定量分析方法。方法：采用显微鉴别和薄层色谱鉴定样品中黄芩、芙蓉叶、姜黄、大黄、黄柏、冰片；采用HPLC法测定黄芩苷含量，色谱柱为C18，以甲醇∶0.4%磷酸溶液(47∶53)为流动相，检测波长280 nm。结果：显微鉴别特征明显、薄层色普清晰，空白样品无干扰；黄芩苷平均回收率为(99±3)%，RSD为3.35 %。结论：该实验简便、可行，重复性好，可用于速效消炎膏质量控制。
목적：탐토속효소염고적정성정량분석방법。방법：채용현미감별화박층색보감정양품중황금、부용협、강황、대황、황백、빙편；채용HPLC법측정황금감함량，색보주위C18，이갑순∶0.4%린산용액(47∶53)위류동상，검측파장280 nm。결과：현미감별특정명현、박층색보청석，공백양품무간우；황금감평균회수솔위(99±3)%，RSD위3.35 %。결론：해실험간편、가행，중복성호，가용우속효소염고질량공제。
AIM: To probe the quanlity and control of Suxiao Xiaoyan Gao. METHODS: The microscopy and TLC were applied to identify Scutellaria baicalensis; Hibiscus mutabilis; Curcuma longa; Rheum palmatum; Phellodendron chinese and borneol. The HPLC on C18column was used to determine the content of baicalin in Suxiao Xiaoyan Gao. Mobile phase was methanol∶0.4% phosphoric acid solution(47∶53). Detection wavelength was 280 nm. RESULTS： The micro-character and thin-layer chromatography was clear with no disturbance of negative sample. The average recovery of baicalin was (99±3)%, RSD was 3.35%. CONCLUSION: The method is simple and feasible. Its repetition is well. It can be used as a quality control method of Suxiao Xiaoyan Gao.