CAJ | 학술논문

采用现代分离技术和方法,从延胡索根茎中分离得到17个化合物,通过波谱分析鉴定其结构.包括11个生物碱类化合物,二氢白屈菜红碱(1)、去氢紫堇碱(2)、四氢非洲防己胺(3)、异紫堇球碱(4)、紫堇碱(5)、四氢黄连碱(6)、药根碱(7)、黄连碱(8)、小檗碱(12)、巴马汀(13)和延胡索乙素(14)；2个蒽醌类化合物,大黄素(9)和大黄素甲醚(10)；1个三萜类化合物,即3β-羟基-齐墩果烷-11,13(18)-二烯-28-酸(11)和3个甾醇类化合物,豆甾醇(15)β-谷甾醇(16)和胡萝卜苷(17).其中,化合物9～11首次从该属植物中分离得到,1首次从该种中分离得到.
채용현대분리기술화방법,종연호색근경중분리득도17개화합물,통과파보분석감정기결구.포괄11개생물감류화합물,이경백굴채홍감(1)、거경자근감(2)、사경비주방기알(3)、이자근구감(4)、자근감(5)、사경황련감(6)、약근감(7)、황련감(8)、소벽감(12)、파마정(13)화연호색을소(14)；2개은곤류화합물,대황소(9)화대황소갑미(10)；1개삼첩류화합물,즉3β-간기-제돈과완-11,13(18)-이희-28-산(11)화3개치순류화합물,두치순(15)β-곡치순(16)화호라복감(17).기중,화합물9～11수차종해속식물중분리득도,1수차종해충중분리득도.
Seventeen compounds have been isolated from Corydalis yanhusuo W.T.Wang.Their structures were deduced on the basts of their physicochemical properties and spectroscopic data.These compounds,including eleven alkaloids,two anthraquinones,a triterpenoid and three steroids,were identified as dihydrochelerythrine ( 1 ),dehydrocorydaline (2),tetrahydrocolumbamine (3),isocorrybulbine (4),corydaline (5),tetrahydrocoptisine (6),jatrorrhizine (7),coptisine (8),emodin (9),physcion ( 10 ),3β-hydroxy-olean-11,13 ( 18 ) -dien-28-oic acid ( 11 ),berberine ( 12 ),palmatine ( 13 ),tetrahydropalmatine (14),stigmasterol ( 15 ),β-sitosterol ( 16 ),and daucosterol ( 17 ).Compounds 9-11 were isolated from genus Corydalis for the first time,and 1 was firstly isolated from this species.