CAJ | 학술논문

以天然产物异黄酮与氨基硫脲为原料,在碱性条件下乙醇为溶剂,合成了10种苯基苄基酮缩氨基硫脲化合物.此方法操作简便、条件温和、且产率较高,是合成苯基苄基缩氨基硫脲的一种简便实用的方法.采用IR,~1H NMR,~(13)CNMR和元素分析对这10种化合物结构进行了表征.
이천연산물이황동여안기류뇨위원료,재감성조건하을순위용제,합성료10충분기변기동축안기류뇨화합물.차방법조작간편、조건온화、차산솔교고,시합성분기변기축안기류뇨적일충간편실용적방법.채용IR,~1H NMR,~(13)CNMR화원소분석대저10충화합물결구진행료표정.
Using natural product isoflavones and thiosemicarbazide as starting materials, ten phenyl-benzylketone thiosemicarbazone derivatives were synthesized from the solution of alkali alcohol.This method is a convenient and efficient way to the synthesis of thiosemicarbazones based on isoflavones and thiosemicarbazide, which has several advantages such as simple operation, short reaction time, mild conditions and high yields. The structures of the ten thiosemicarbazones were identified by IR, NMR spectra and elemental analysis.