CAJ | 학술논문

以丙烯酸和环己醇为原料合成丙烯酸环己酯,考察了不同催化剂、阻聚剂用量、催化剂用量、醇酸比及反应时间对丙烯酸转化率和选择性的影响,得到的最佳工艺条件为：催化剂为甲基苯磺酸,用量为1%,醇酸比为1.5,阻聚剂为3‰,带水剂用量为5%,丙烯酸转化率大于90%,选择性大于80%.
이병희산화배기순위원료합성병희산배기지,고찰료불동최화제、조취제용량、최화제용량、순산비급반응시간대병희산전화솔화선택성적영향,득도적최가공예조건위：최화제위갑기분광산,용량위1%,순산비위1.5,조취제위3‰,대수제용량위5%,병희산전화솔대우90%,선택성대우80%.
Cyclohexyl acrylate is synthesized with Acrylic acid and cyclohexanol.The amount of catalyst and the different catalysts,the amount of inhibitor and catalyst,the ratio of cyclohexanol to Acrylic acid and reaction time was investigated.The results indicated that： The catalyst of benzenesulfonic acid was 1%;The ratio of cyclohexanol to Acrylic acid was 1.5,inhibitor was 3 ‰,the solvent was 5%;the conversion of acrylic acid is above 90% and the selectivity is above 80%.