广东化工
廣東化工
엄동화공
GUANGDONG CHEMICAL INDUSTRY
2012年
3期
52-52,47
,共2页
李洪侠%綦菲%栾波%吴文雷%刘英贤
李洪俠%綦菲%欒波%吳文雷%劉英賢
리홍협%기비%란파%오문뢰%류영현
氰氟虫腙%中间体%对三氟甲氧基苯胺基甲酸乙酯%合成
氰氟蟲腙%中間體%對三氟甲氧基苯胺基甲痠乙酯%閤成
청불충종%중간체%대삼불갑양기분알기갑산을지%합성
metaflumizone: intermediate%4-trifluoro methoxy Phenyl Ethyl carbamate: synthesis
文章介绍了杀虫剂氰氟虫腙的发展状况,介绍了一种氰氟虫腙的中间体对三氟甲氧基苯胺基甲酸乙酯的合成方法。该方法以水为溶剂体系合成对三氟甲氧基苯胺基甲酸乙醑.含量大于96%,收率超过97%,具有操作简单、三废少、利于环境保护等特点,生产成本低,适宜工业化人生产。
文章介紹瞭殺蟲劑氰氟蟲腙的髮展狀況,介紹瞭一種氰氟蟲腙的中間體對三氟甲氧基苯胺基甲痠乙酯的閤成方法。該方法以水為溶劑體繫閤成對三氟甲氧基苯胺基甲痠乙醑.含量大于96%,收率超過97%,具有操作簡單、三廢少、利于環境保護等特點,生產成本低,適宜工業化人生產。
문장개소료살충제청불충종적발전상황,개소료일충청불충종적중간체대삼불갑양기분알기갑산을지적합성방법。해방법이수위용제체계합성대삼불갑양기분알기갑산을서.함량대우96%,수솔초과97%,구유조작간단、삼폐소、리우배경보호등특점,생산성본저,괄의공업화인생산。
The paper describes the development situation of insecticide metaflumizone, Describes a synthetic method of 4-trifluoro methoxy Phenyl Ethyl carbamate(the intermediate of metaflumizone). It synthesis 4-trifluoro methoxy in solvent system of water, the purity of the product was greater than 96 % and the yield was greater than 97 %. Having the advantages of simple operation, less three wastes, environmental protection and other features. The production cost is lower, it was suitable for industrialized production.