林产化学与工业
林產化學與工業
림산화학여공업
CHEMISTRY AND INDUSTRY OF FOREST PRODUCTS
2007年
z1期
37-40
,共4页
司传领%邓小娟%刘忠%金辰奎%裵映寿
司傳領%鄧小娟%劉忠%金辰奎%裵映壽
사전령%산소연%류충%금신규%배영수
泡桐(原变种)%苯丙素苷%抑菌性
泡桐(原變種)%苯丙素苷%抑菌性
포동(원변충)%분병소감%억균성
Paulownia tomentosa(Thunb.) Steud. var. tomentosa.%phenylpropanoid glycoside%antibacterial activity
研究了泡桐(原变种)果实的化学成分.采用Sephadex LH-20柱色谱及薄层色谱等方法进行分离,从其70%丙酮提取物水溶性部分分离得到4种苯丙素苷化合物,经波谱分析及理化性质分析,化合物分别鉴定为:毛蕊花苷(1)、异毛蕊花苷(2)、campneosideⅡ(3)和isocampneosideⅡ(4).化合物1和2首次从该植物中得到.抑菌活性试验结果表明,泡桐(原变种)果实中分离得到的苯丙素苷化合物、丙酮提取物、乙酸乙酯溶及水溶性部分具有较高的抑菌活性,其中,对革兰氏阳性菌中表皮葡萄球菌的抑制能力最强.
研究瞭泡桐(原變種)果實的化學成分.採用Sephadex LH-20柱色譜及薄層色譜等方法進行分離,從其70%丙酮提取物水溶性部分分離得到4種苯丙素苷化閤物,經波譜分析及理化性質分析,化閤物分彆鑒定為:毛蕊花苷(1)、異毛蕊花苷(2)、campneosideⅡ(3)和isocampneosideⅡ(4).化閤物1和2首次從該植物中得到.抑菌活性試驗結果錶明,泡桐(原變種)果實中分離得到的苯丙素苷化閤物、丙酮提取物、乙痠乙酯溶及水溶性部分具有較高的抑菌活性,其中,對革蘭氏暘性菌中錶皮葡萄毬菌的抑製能力最彊.
연구료포동(원변충)과실적화학성분.채용Sephadex LH-20주색보급박층색보등방법진행분리,종기70%병동제취물수용성부분분리득도4충분병소감화합물,경파보분석급이화성질분석,화합물분별감정위:모예화감(1)、이모예화감(2)、campneosideⅡ(3)화isocampneosideⅡ(4).화합물1화2수차종해식물중득도.억균활성시험결과표명,포동(원변충)과실중분리득도적분병소감화합물、병동제취물、을산을지용급수용성부분구유교고적억균활성,기중,대혁란씨양성균중표피포도구균적억제능력최강.
Column chromatographic study on the aqueous acetone (70 % ) extract of Paulownia tomentosa(Thunb.) Steud. var. tomentosa fruit led to the isolation of 4 phenylpropanoid glycosides and their structures were determined as verbascoside (1), isoverbascoside (2) campneoside Ⅱ (3) and isocampneoside Ⅱ (4) by chemical and spectral analyses. Compounds 1-2 were isolated from the title plant for the first time. The study on antibacterial activity showed that the isolated compounds, acetone extract, EtOAc and H2O fractions exhibited significant inhibition,particularly against Staphylococcus epidermidis.