四川环境
四川環境
사천배경
2011年
6期
47-50
,共4页
熊杰%孙方中%罗晓慧%王丽萍
熊傑%孫方中%囉曉慧%王麗萍
웅걸%손방중%라효혜%왕려평
四氯化碳%四氯乙烯%代替%分析%油类
四氯化碳%四氯乙烯%代替%分析%油類
사록화탄%사록을희%대체%분석%유류
Carbon tetrachloride%tetrachloroethylene%instead of%analysis%oil
通过使用四氯乙烯代替四氯化碳测定水中油类物质的对比实验,得到如下结论:四氯乙烯作萃取剂时,标准曲线线性相关系数为0.9999,检出限为0.336mg/L,精密度和准确度符合质控要求。但标准曲线方程的斜率较差,在分析浓度较低的样品时,准确度相对误差较大,萃取回收率不高。由此可以看出,使用四氯乙烯分析油类物质的局限性较大,分析方法还需进一步研究。
通過使用四氯乙烯代替四氯化碳測定水中油類物質的對比實驗,得到如下結論:四氯乙烯作萃取劑時,標準麯線線性相關繫數為0.9999,檢齣限為0.336mg/L,精密度和準確度符閤質控要求。但標準麯線方程的斜率較差,在分析濃度較低的樣品時,準確度相對誤差較大,萃取迴收率不高。由此可以看齣,使用四氯乙烯分析油類物質的跼限性較大,分析方法還需進一步研究。
통과사용사록을희대체사록화탄측정수중유류물질적대비실험,득도여하결론:사록을희작췌취제시,표준곡선선성상관계수위0.9999,검출한위0.336mg/L,정밀도화준학도부합질공요구。단표준곡선방정적사솔교차,재분석농도교저적양품시,준학도상대오차교대,췌취회수솔불고。유차가이간출,사용사록을희분석유류물질적국한성교대,분석방법환수진일보연구。
By conducting contrast experiments for determination of oil in water using tetrachloroethylene instead of carbon tetrackloride, it concluded that when tetraehloroethylene was used as extractant, the liner correlation coefficient was 0. 9999, detection limit was 0. 336mg/L and the precision and accuracy met the requirements of the quality control. However the slope of the standard curve equation was low. When samples with low concentration were analyzed, the relative errors of accuracy were low and the extraction recovery was poor. It concluded that there were still limitations to use tetrachloreethylene for determination of oil in water, so the method needs further studies.