功能材料
功能材料
공능재료
JOURNAL OF FUNCTIONAL MATERIALS
2009年
11期
1818-1821
,共4页
米春旭%贺俊艳%秦敬玉%潘少鹏
米春旭%賀俊豔%秦敬玉%潘少鵬
미춘욱%하준염%진경옥%반소붕
Fe_(78)Si_9B_(13)非晶合金%直流四端接线法%等温退火%晶化
Fe_(78)Si_9B_(13)非晶閤金%直流四耑接線法%等溫退火%晶化
Fe_(78)Si_9B_(13)비정합금%직류사단접선법%등온퇴화%정화
Fe_(78)Si_9B(13)%DCFT%isothermal annealing%crystallization
采用直流四端接线法测量Fe_(78)Si_9B_(13)非晶合金在等温退火和升温过程中的电阻变化.结果表明,当温度高于693K时非晶结构易被热效应所影响.与DSC法相比较,直流电阻四端接线法的优点是能够反映出晶化的形核阶段.但是R-T曲线上所反映的晶化第二阶段的特征不明显,晶化第二阶段产物Fe_2B的电阻率比第一阶段产物Fe_3B的高可能是造成这一现象的原因.
採用直流四耑接線法測量Fe_(78)Si_9B_(13)非晶閤金在等溫退火和升溫過程中的電阻變化.結果錶明,噹溫度高于693K時非晶結構易被熱效應所影響.與DSC法相比較,直流電阻四耑接線法的優點是能夠反映齣晶化的形覈階段.但是R-T麯線上所反映的晶化第二階段的特徵不明顯,晶化第二階段產物Fe_2B的電阻率比第一階段產物Fe_3B的高可能是造成這一現象的原因.
채용직류사단접선법측량Fe_(78)Si_9B_(13)비정합금재등온퇴화화승온과정중적전조변화.결과표명,당온도고우693K시비정결구역피열효응소영향.여DSC법상비교,직류전조사단접선법적우점시능구반영출정화적형핵계단.단시R-T곡선상소반영적정화제이계단적특정불명현,정화제이계단산물Fe_2B적전조솔비제일계단산물Fe_3B적고가능시조성저일현상적원인.
The direct current four-terminal (DCFT) method was applied for the investigation on isothermal annealing and crystallization of amorphous Fe_(78)Si_9B(13) ribbons. The results show that thermal effect can influence the amorphous structure easily at the temperature above 693K. The DCFT method has the advantage to reveal the nucleation stage during crystallization over the DSC method. However, the feature about the second stage of the crystallization in R-T curve is more inconspicuous than that in DSC curve. We then suggest that the resistivity of the crystallization product Fe_2B of the second stage is higher than that (Fe_3B) of the first stage.