广州化工
廣州化工
엄주화공
GUANGZHOU CHEMICAL INDUSTRY AND TECHNOLOGY
2011年
23期
106-108
,共3页
胥亚云%仲苏林%吴建兰%曹新梅%章东生%曹雄飞
胥亞雲%仲囌林%吳建蘭%曹新梅%章東生%曹雄飛
서아운%중소림%오건란%조신매%장동생%조웅비
三唑磷%阿维菌素%高效液相色谱%分析
三唑燐%阿維菌素%高效液相色譜%分析
삼서린%아유균소%고효액상색보%분석
triazophos%abamectin%HPLC%analysis
建立了一种高效液相色谱法（HPLC）同时测定混剂中三唑磷和阿维菌素含量的方法。本文采用Eclipse XDB C18不锈钢柱,以甲醇、乙腈和水为流动相,使用梯度洗脱程序,在245 nm波长下,同时分离测定三唑磷.阿维菌素10.5%微囊悬浮剂中的有效成分。结果表明,三唑磷和阿维菌素的线性相关系数分别为0.9999和0.9997;标准偏差分别为0.029、0.060;变异系数分别为0.36%、2.37%;平均回收率分别为99.59%、99.83%。
建立瞭一種高效液相色譜法（HPLC）同時測定混劑中三唑燐和阿維菌素含量的方法。本文採用Eclipse XDB C18不鏽鋼柱,以甲醇、乙腈和水為流動相,使用梯度洗脫程序,在245 nm波長下,同時分離測定三唑燐.阿維菌素10.5%微囊懸浮劑中的有效成分。結果錶明,三唑燐和阿維菌素的線性相關繫數分彆為0.9999和0.9997;標準偏差分彆為0.029、0.060;變異繫數分彆為0.36%、2.37%;平均迴收率分彆為99.59%、99.83%。
건립료일충고효액상색보법（HPLC）동시측정혼제중삼서린화아유균소함량적방법。본문채용Eclipse XDB C18불수강주,이갑순、을정화수위류동상,사용제도세탈정서,재245 nm파장하,동시분리측정삼서린.아유균소10.5%미낭현부제중적유효성분。결과표명,삼서린화아유균소적선성상관계수분별위0.9999화0.9997;표준편차분별위0.029、0.060;변이계수분별위0.36%、2.37%;평균회수솔분별위99.59%、99.83%。
A method for the separation and determination of Triazophos·Abamectin 10.5% CS by HPLC was described using methanol,acetonitrile and water as mobile phase with gradient program,Eclipse XDB C18 column and DAD at 245 nm.The results showed that the linear correlation coeficients for Triazophos and Abamectin were 0.9999 and 0.9997,the standard deviations were 0.029 and 0.060,the variation coeffients were 0.36% and 2.37%,and the average recovery was 99.59% and 99.83%,respectively.
