绵阳师范学院学报
綿暘師範學院學報
면양사범학원학보
JOURNAL OF MIANYANG NORMAL UNIVERSITY
2011年
8期
49-51
,共3页
杨葵华%黎国兰%谢丽%邓文文
楊葵華%黎國蘭%謝麗%鄧文文
양규화%려국란%사려%산문문
燕麦片%微量元素%火焰原子吸收光谱法
燕麥片%微量元素%火燄原子吸收光譜法
연맥편%미량원소%화염원자흡수광보법
Oatmeal%trace elements%flame atomic absorption spectrometry
采用HNO3-HClO4(4+1)湿法消解样品,用火焰原子吸收光谱法测定燕麦片中铁、锰、铜、锌的含量。测得铁、锰、铜、锌的回收率分别在98%~100%、99%~101%9、8%~99%9、6%~101%之间。平均回收率为96%~101%,RSD为0.3%~0.9%,表明该方法准确可靠。
採用HNO3-HClO4(4+1)濕法消解樣品,用火燄原子吸收光譜法測定燕麥片中鐵、錳、銅、鋅的含量。測得鐵、錳、銅、鋅的迴收率分彆在98%~100%、99%~101%9、8%~99%9、6%~101%之間。平均迴收率為96%~101%,RSD為0.3%~0.9%,錶明該方法準確可靠。
채용HNO3-HClO4(4+1)습법소해양품,용화염원자흡수광보법측정연맥편중철、맹、동、자적함량。측득철、맹、동、자적회수솔분별재98%~100%、99%~101%9、8%~99%9、6%~101%지간。평균회수솔위96%~101%,RSD위0.3%~0.9%,표명해방법준학가고。
To preprocess samples of oatmeal with HNO3-HClO4(4+1) wet digestion,the contents of Fe,Mn,Cu,Zn in oatmeal can be determined by flame atomic absorption spectrometry,obtaining the recovery rate of 98%~100% for Fe,99%~101% for Mn,98%~99% for Cu,96%~101% for Zn.,and the average rate is 96%~101%,RSD is 0.3%~0.9%.The result of this experiment shows that the method is reliable and accurate for the test.