中药材
中藥材
중약재
JOURNAL OF CHINESE MEDICINAL MATERIALS
2001年
1期
36-37
,共2页
陈汝贤%王海燕%许鸿章%徐桂云%常理文
陳汝賢%王海燕%許鴻章%徐桂雲%常理文
진여현%왕해연%허홍장%서계운%상리문
岷当归%多糖%毛细管气相色谱
岷噹歸%多糖%毛細管氣相色譜
민당귀%다당%모세관기상색보
从岷当归Angelicasinensis(Oliv)Diels中分离得到两个多糖组分X-C-3-Ⅲ和X-C-3-Ⅳ，凝胶色谱法测得分子量分别为85000和65765，水解后利用硅烷化和毛细管气相色谱法分析确定X-C-3-Ⅲ和X-C-3-Ⅳ的糖基组成为半乳糖、阿拉伯糖、鼠李糖、葡萄糖醛酸和半乳糖醛酸，摩尔比分别为24.3:15.8:4.2:3.1:52.6和12.6:10.7:7.2:8.3:61.2。
從岷噹歸Angelicasinensis(Oliv)Diels中分離得到兩箇多糖組分X-C-3-Ⅲ和X-C-3-Ⅳ，凝膠色譜法測得分子量分彆為85000和65765，水解後利用硅烷化和毛細管氣相色譜法分析確定X-C-3-Ⅲ和X-C-3-Ⅳ的糖基組成為半乳糖、阿拉伯糖、鼠李糖、葡萄糖醛痠和半乳糖醛痠，摩爾比分彆為24.3:15.8:4.2:3.1:52.6和12.6:10.7:7.2:8.3:61.2。
종민당귀Angelicasinensis(Oliv)Diels중분리득도량개다당조분X-C-3-Ⅲ화X-C-3-Ⅳ，응효색보법측득분자량분별위85000화65765，수해후이용규완화화모세관기상색보법분석학정X-C-3-Ⅲ화X-C-3-Ⅳ적당기조성위반유당、아랍백당、서리당、포도당철산화반유당철산，마이비분별위24.3:15.8:4.2:3.1:52.6화12.6:10.7:7.2:8.3:61.2。
Polysaccharides X-C-3-Ⅲ had been obtained from Angelica sinensis(Oliv) Diels. Their average MW were determined to be 85000 and 65765 by gel chromatography. after the hydrolysates of X-C-3-Ⅲ and X-C-3-Ⅳ, the compositions of them were identifed by si lanization method and capillary gas chromatography. X-C-3-Ⅲ and X-C-3-Ⅳ are composed of galacose,arabinose, rhamnose,glucuronic acid and galacturonic acid. The molar ratio of those sugars were determined as 24.3: 15.8:4.2:3. 1:52.6 and 12.6: 10.7:7.2:8.3:61.2, respectively.
