化学试剂
化學試劑
화학시제
CHEMICAL REAGENTS
2009年
11期
889-891
,共3页
刘艳凤%花成文%苟小锋%赵军龙
劉豔鳳%花成文%茍小鋒%趙軍龍
류염봉%화성문%구소봉%조군룡
三聚氯氰%三嗪化合物%杂环蕃%合成%表征
三聚氯氰%三嗪化閤物%雜環蕃%閤成%錶徵
삼취록청%삼진화합물%잡배번%합성%표정
cyanuric chloride%triazine compound%heterocyclophane%synthesis%characterization
以三聚氯氰、甲胺、乙胺、二甲胺、苯酚、二(4-氨基苯基)醚为原料,经取代、傅克反应和成环作用合成了一类新的含三嗪环的杂环蕃,并通过 ~1HNMR、IR和MALDI-TOFMS对其结构进行了表征.
以三聚氯氰、甲胺、乙胺、二甲胺、苯酚、二(4-氨基苯基)醚為原料,經取代、傅剋反應和成環作用閤成瞭一類新的含三嗪環的雜環蕃,併通過 ~1HNMR、IR和MALDI-TOFMS對其結構進行瞭錶徵.
이삼취록청、갑알、을알、이갑알、분분、이(4-안기분기)미위원료,경취대、부극반응화성배작용합성료일류신적함삼진배적잡배번,병통과 ~1HNMR、IR화MALDI-TOFMS대기결구진행료표정.
Some novel heterocyclophanes containing 1,3, 5-tri-azine were synthesized from cyanuric chloride, aniline, ethy-lamine, dimethylamine, phenol and di (4-aminophenyl) ether via substitution, Friedel-Crafts alkylation and cyclization, and their structures were characterized by ~1HNMR, IR and MALDI-TOF-MS techniques.
