CAJ | 학술논문

目的建立一种快速有效的分析方法,达到鉴定淫羊藿及人参复方产品中黄酮苷类及人参皂苷类成分,并测定各成分含量的目的,最终控制复方中淫羊藿及人参的比例.方法通过反相液相色谱,对包括药典所收载的淫羊藿药材及其产品进行分析.淫羊藿中的主要黄酮苷类成分,以淫羊藿定A、淫羊藿定B、淫羊藿定C、淫羊藿苷为对照品;对主要的人参皂苷类成分,以人参皂苷Rg1、Re、Rf、Rb1、Rb2、Rd为对照品.结果在同一色谱条件下,对主要黄酮苷类及人参皂苷类成分均可同时测定且分离良好.结论该方法适用于淫羊藿、人参及其复方产品中淫羊藿黄酮苷类、人参皂苷类成分的定性、定量分析.
목적건립일충쾌속유효적분석방법,체도감정음양곽급인삼복방산품중황동감류급인삼조감류성분,병측정각성분함량적목적,최종공제복방중음양곽급인삼적비례.방법통과반상액상색보,대포괄약전소수재적음양곽약재급기산품진행분석.음양곽중적주요황동감류성분,이음양곽정A、음양곽정B、음양곽정C、음양곽감위대조품;대주요적인삼조감류성분,이인삼조감Rg1、Re、Rf、Rb1、Rb2、Rd위대조품.결과재동일색보조건하,대주요황동감류급인삼조감류성분균가동시측정차분리량호.결론해방법괄용우음양곽、인삼급기복방산품중음양곽황동감류、인삼조감류성분적정성、정량분석.
Aim To develop a rapid, effective method for the determination of flavonoids and ginsenosides in one injection and evaluate the flavonoids and ginsenosides content to control the ratio of Epimedium and Ginseng herbs in botanicalcombinations. Methods The quality evaluation was determinatted using reversed-phase high performance liquid chromatog raphy (HPLC), referred by the major flavonoids from Epimedium, epimedin A, epimedin B, epimedin C, and icariin as thestandards, and the major ginsenosides Rg1 , Re, Rf, Rb1 , Rb2, and Rd as the standards, included Epimedium brevicornumMaxim., E. sagittatum (Sieb. et Zucc) Maxim., E. koreanum NaKai, P. ginseng C. A. Meyer, P. quinquefoliumL., P. notoginseng and some products containing the above herbs. Results The main flavonoids and ginsenosides couldbe clearly resolved in the single analysis. Conclusion The results can be effectively used in evaluating qualitatively andquantitatively the ration of Epimedium and Ginseng contained products.