天然产物研究与开发
天然產物研究與開髮
천연산물연구여개발
NATURAL PRODUCT RESEARCH AND DEVELOPMENT
2011年
1期
1-5,24
,共6页
杨振民%伊勇涛%高川川%范坚强%胡军%赵明月
楊振民%伊勇濤%高川川%範堅彊%鬍軍%趙明月
양진민%이용도%고천천%범견강%호군%조명월
巴戟天%多糖%结构%FTIR%HPLC%NMR%GC-MS
巴戟天%多糖%結構%FTIR%HPLC%NMR%GC-MS
파극천%다당%결구%FTIR%HPLC%NMR%GC-MS
Morinda officinalis How%polysaccharide%structure%HPLC%NMR%GC-MS
中药巴戟天(Morinda officinalis)的根经过水提、醇沉、脱色和离子交换得到水溶性多糖(MOHP-1),经过FIIR、HPLC、NMR和GC-MS分析,最后确定MOHP-1是由果糖以(2→1)糖苷键连接的菊淀粉性多糖,其结构为α-Glcp(1→2)-[β-Fruf-(2→1)-β-Frucf].
中藥巴戟天(Morinda officinalis)的根經過水提、醇沉、脫色和離子交換得到水溶性多糖(MOHP-1),經過FIIR、HPLC、NMR和GC-MS分析,最後確定MOHP-1是由果糖以(2→1)糖苷鍵連接的菊澱粉性多糖,其結構為α-Glcp(1→2)-[β-Fruf-(2→1)-β-Frucf].
중약파극천(Morinda officinalis)적근경과수제、순침、탈색화리자교환득도수용성다당(MOHP-1),경과FIIR、HPLC、NMR화GC-MS분석,최후학정MOHP-1시유과당이(2→1)당감건련접적국정분성다당,기결구위α-Glcp(1→2)-[β-Fruf-(2→1)-β-Frucf].
A soluble polysaccharide (MOHP-1) was isolated from the roots of Morinda officinalis How via procedures including extraction,precipitation,deprotein,decolor and separation over anion-exchange.On the basis of FTIR,HPLC,NMR and GC-MS analysis after methylation,MOHP-1 was determined as α-Glcp- (1 →2) -[β-Fruf- (2→1)-β-Frucf]n,a polysaccharide with a linear chain of (2→1) linked β-fructofuranosyl residues specifying an inulin-type structure.
