林产化学与工业
林產化學與工業
림산화학여공업
CHEMISTRY AND INDUSTRY OF FOREST PRODUCTS
2011年
3期
60-64
,共5页
李大伟%毕良武%赵振东%李冬梅%刘先章
李大偉%畢良武%趙振東%李鼕梅%劉先章
리대위%필량무%조진동%리동매%류선장
鼠尾草酸%迷迭香%超声波辅助提取
鼠尾草痠%迷迭香%超聲波輔助提取
서미초산%미질향%초성파보조제취
carnosic acid%rosemary (Rosmarinus officinalis L.)%ultrasound-assisted extraction
利用超声波辅助提取法提取迷迭香中的主要生物活性成分鼠尾草酸,分别研究了不同条件对鼠尾草酸提取率的影响.对5.0 g粉碎后的迷迭香叶子进行超声波辅助提取的结果表明,室温较适宜的超声波提取条件是:乙醇质量分数75%、3 g盐酸为酸稳定剂、超声波频率28 kHz、超声波功率200W、超声波提取时间40min、料液比(g:g)1:16.在上述提取条件下,鼠尾草酸的得率可达18.64mg/g.
利用超聲波輔助提取法提取迷迭香中的主要生物活性成分鼠尾草痠,分彆研究瞭不同條件對鼠尾草痠提取率的影響.對5.0 g粉碎後的迷迭香葉子進行超聲波輔助提取的結果錶明,室溫較適宜的超聲波提取條件是:乙醇質量分數75%、3 g鹽痠為痠穩定劑、超聲波頻率28 kHz、超聲波功率200W、超聲波提取時間40min、料液比(g:g)1:16.在上述提取條件下,鼠尾草痠的得率可達18.64mg/g.
이용초성파보조제취법제취미질향중적주요생물활성성분서미초산,분별연구료불동조건대서미초산제취솔적영향.대5.0 g분쇄후적미질향협자진행초성파보조제취적결과표명,실온교괄의적초성파제취조건시:을순질량분수75%、3 g염산위산은정제、초성파빈솔28 kHz、초성파공솔200W、초성파제취시간40min、료액비(g:g)1:16.재상술제취조건하,서미초산적득솔가체18.64mg/g.
Carnosic acid, the key bioactive component, was extracted from leaves of rosemary (Rosmarinus officinalis L.)using ultrasound-assisted extraction. The different factors such as ethanol concentration, variety of acid stabilizer, acid stabilizer dosage, ultrasonic frequency, ultrasonic power, ultrasonic extraction time and the solid-liquid ratio were studied. The content variations of carnosol, rosmarinic acid, oleanolic acid and ursolic acid were also examined.The experimental results for 5.0 g rosemary leaves showed that the optimum ultrasonic extraction conditions at room temperature were: ethanol solution concentration 75 %, acid stabilizer 3 g hydrochloric acid, ultrasonic frequency 28 kHz, ultrasonic power 200 W, ultrasonic extraction time 40 min, solid-liquid ratio(g: g)1: 16. The extraction rate of carnosic acid reached 18.64 mg/g under the above extraction conditions.