解放军药学学报
解放軍藥學學報
해방군약학학보
PHARMACEUTICAL JOURNAL OF CHINESE PEOPLE'S LIBERATION ARMY
2001年
2期
108-108，116
,共2页
邓丽萍%胡琳%李仙逸%袁海龙%肖小河
鄧麗萍%鬍琳%李仙逸%袁海龍%肖小河
산려평%호림%리선일%원해룡%초소하
高效液相色谱法%肝得宁胶囊%连翘苷
高效液相色譜法%肝得寧膠囊%連翹苷
고효액상색보법%간득저효낭%련교감
目的建立肝得宁胶囊中连翘苷的HPLC含量法测定。方法固定相：RP-C18柱，流动相：甲醇-水(50∶50)，检测波长280nm。结果连翘苷含量测定线性范围0.24～2.40μg,加样回收率为94.74%,RSD为2.74%。结论本法可用于肝得宁胶囊中连翘苷的质量控制。
目的建立肝得寧膠囊中連翹苷的HPLC含量法測定。方法固定相：RP-C18柱，流動相：甲醇-水(50∶50)，檢測波長280nm。結果連翹苷含量測定線性範圍0.24～2.40μg,加樣迴收率為94.74%,RSD為2.74%。結論本法可用于肝得寧膠囊中連翹苷的質量控製。
목적건립간득저효낭중련교감적HPLC함량법측정。방법고정상：RP-C18주，류동상：갑순-수(50∶50)，검측파장280nm。결과련교감함량측정선성범위0.24～2.40μg,가양회수솔위94.74%,RSD위2.74%。결론본법가용우간득저효낭중련교감적질량공제。
Aim To establish the determination method of phillyrin in Gandening capsule.Methods HPLC condition:C18 column as solid phase,methanal-water(50∶50) as mobile phase and detective wavelength at 280nm.Results Phillyrin's linear range is 0.24～2.40μg,added standard material recovery rate is 94.74% and RSD is 2.74%.Conclusion The method can be used in the quality control of Gandening capsule.
