宜春学院学报
宜春學院學報
의춘학원학보
JOURNAL OF YICHUN UNIVERSITY
2011年
12期
11-12,90
,共3页
碱式碳酸铜%制备%改进
堿式碳痠銅%製備%改進
감식탄산동%제비%개진
Basis Carbonate Copper%Prepare%Improvement
探讨了无机化学实验中碱式碳酸铜制备的改进方法。采用CuS04和Na2CO,为原料进行制备,确定了最佳实验条件为nCuS04/nNa2C03=1:1,T=60℃,终点溶液pH=8.5,静置48h,反加(硫酸铜溶液加入到碳酸钠溶液)。通过元素分析、红外光谱分析、X—RD等手段确定了该方法制备出了高纯度的碱式碳酸铜。
探討瞭無機化學實驗中堿式碳痠銅製備的改進方法。採用CuS04和Na2CO,為原料進行製備,確定瞭最佳實驗條件為nCuS04/nNa2C03=1:1,T=60℃,終點溶液pH=8.5,靜置48h,反加(硫痠銅溶液加入到碳痠鈉溶液)。通過元素分析、紅外光譜分析、X—RD等手段確定瞭該方法製備齣瞭高純度的堿式碳痠銅。
탐토료무궤화학실험중감식탄산동제비적개진방법。채용CuS04화Na2CO,위원료진행제비,학정료최가실험조건위nCuS04/nNa2C03=1:1,T=60℃,종점용액pH=8.5,정치48h,반가(류산동용액가입도탄산납용액)。통과원소분석、홍외광보분석、X—RD등수단학정료해방법제비출료고순도적감식탄산동。
It is studied for the Improvement and exploration of the prepared experiment of the basis carbonate copper in inorganic chemistry. CuSO4 and Na2CO3 as raw material to prepare the Basis Carbonate Copper. The results show that the optimum reaction conditions are as follows : reaction temperature is 60℃, the ratio of n CuSO4/n Na2 CO3 is 1 : 1, and pH is about 8. 5, standing time is 48h, the approach is add -back (copper sulfate solution into sodium carbonate solution) . By elemental analysis, IR and X -RD, high purity basic copper carbonate is synthesized