CAJ | 학술논문

以钼酸钠（Na2MoO4）、水合肼（N2H2·H2O）、硫代乙酰胺（CH3CSNH2）和盐酸（HCl）为原材料。利用气泡液膜法合成工艺制备纳米级的二硫化钼。采用XPS、SEM、激光粒度分析仪对合成产物的组成、包覆效果、形貌和粒径进行了表征。测定了合成产物的表面能。结果表明采用气泡液膜法合成工艺制备得到油酸包覆、分散均匀、无团聚、平均粒径为70nm的纳米级的二硫化钼，且合成产物粒子表面能大大降低，仅为5．286mN／m。
이목산납（Na2MoO4）、수합정（N2H2·H2O）、류대을선알（CH3CSNH2）화염산（HCl）위원재료。이용기포액막법합성공예제비납미급적이류화목。채용XPS、SEM、격광립도분석의대합성산물적조성、포복효과、형모화립경진행료표정。측정료합성산물적표면능。결과표명채용기포액막법합성공예제비득도유산포복、분산균균、무단취、평균립경위70nm적납미급적이류화목，차합성산물입자표면능대대강저，부위5．286mN／m。
Nano- molybdenum disulfide was synthesized with sodium molybdate, hydrazine hydrate, thioacetamide, hydrochloric acid by using the bubble - liquid film synthesizing method. The obtained products were characterized by XPS,SEM, particle size analysis, the surface energy of product was also detected. The results showed that nano -molybdenum disulfide prepared by the bubble -liquid film synthesizing method was coated with oleic acid, uniformly dispersed, less aggregation. Its particle size was about 70nm, which surface energy was only 5. 286 mN/m.